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← Document results/DEP Box 04/524 1/22/02
Document / 77 pages

VOCs GC/MS analysis results, Jan 22-23 2002

Machine-extracted title · confidence 90%

Laboratory report showing volatile organic compound analysis results for sample AE01036 processed on January 22 and 23, 2002.

NYC-WTC_000003249–000003325

Folder label: “524 1/22/02”

Page image
Scanned page image, NYC-WTC_000003315
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\02JAN22\01040.D Vial: 17 Acq On : 22 Jan 2002 10:34 pm Operator: Sample : nyc Inst : 210 Misc : January 22, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\HP010802.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L

Peak Number 3 Cyclotrisiloxane, hexamethyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T. --------------------------------------------------------------------- 21.10 0.11 ug/L 29895 1,4-DIFLUOROBENZENE 17.56

Hit# of 5 Tentative ID MW MolForm CAS# Qual --------------------------------------------------------------------- 1 Cyclotrisiloxane, hexamethyl- 222 C6H18O3Si3 000541-05-9 83 2 Arsenous acid, tris(trimethylsilyl) 342 C9H27AsO3Si3 055429-29-3 56 3 Hexahydropyridine, 1-methyl-4-[4,5- 207 C12H17NO2 000000-00-0 53 4 1H-Indole, 1-methyl-2-phenyl- 207 ClSH13N 003558-24-5 42 9 (21.105 min): 01040.D (-) m Z 27

5000

40 96 133 20.80 21.00 21.20 21.40 191 59 75 161 m Z 2Os.Os 18.79w > 40 60 80 100 120 14 240 260 280 dance #7058'

5000

75 I T I I I I I 119 13314716311 191

80 100 120 140 160 1 ester

5000

73 105 133 44 147 191 223 239 327 > 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 dance #24610: Hexahydropyridine, 1-methyl-4-[4,5-dihydroxyphenyl]- 2 7 20.80 21.00 21.20 21.40 70 42 m z 1.33.05 11.22 97 5000

136 123 150 192

60 80 100 120 140 160 180 200 220 240 260 280 300 320 20.80 21.00 21.20 21.40

01040.D HP010802.M Wed Jan 23 09:51:34 2002 Page 3 NYC-WTC 000003315

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NYC-WTC_000003315Source: NYC Law Department, mirrored locally

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