VOCs GC/MS analysis results, Jan 10-16 2002

NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed) Data File : C:\HPCHEM\1\DATA\02JAN10\0110R40.D Vial: 3 Acq On : 10 Jan 2002 1:36 pm Operator: 206-bh Sample : as /3 .1► 4 , Inst : GC/ MS Ins Misc /`~' Multiply: 1.00 MS Integration Params: LSCINT.P Quant Time: Jan 11 9:02 2002 Quant Results File: HP010402.RES Quant Method : C:\HPCHEM\1\METHODS\HP010402.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Last Update : Thu Jan 10 10:17:54 2002 Response via : Initial Calibration DataAcq Meth : HP121001

Internal Standards R.T. Qlon Response Conc Units Dev(Min) 1) 1,4-DIFLUOROBENZENE 14.46 114 631223 5.00 ug/L 0.07 22) CHLOROBENZENE-D5 21.05 117 721977 5.00 ug/L 0.05 50) 1,4-DIFHLOROBENZENE-D4 26.21 152 620538 5.00 ug/L 0.05 System Monitoring Compounds 2) 1,2-DICHLOROETHANE-D4 13.67 65 208715 4.55 ug/L 0.05 Spiked Amount 5.000 Recovery = 91.00% 3) 4-BROMOFLUOROBENZENE 23.62 174 348062 6.13 ug/L 0.05 Spiked Amount 5.000 Recovery = 122.60% 23) TOLUENE-D8 17.78 98 826294 4.51 ug/L 0.07 Spiked Amount 5.000 Recovery = 90.20% Target Compounds Qvalue 4) DICHLORODIFLUOROMETHANE 4.48 85 1200391 40.47 ug/L 100 5) CHLOROMETHANE 5.00 50 1375579 52.49 ug/L 99 6) VINYL CHLORIDE 5.14 62 1116985 40.52 ug/L 99 7) BROMOMETHANE 6.08 94 1089549 57.34 ug/L 98 8) CHLOROETHANE 6.21 64 842057 63.78 ug/L 99 9) TRICHLOROFLUOROMETHANE 6.77 101 2000000 55.69 ug/L 99 10) ACETONE 7.69 43 174691 34.82 ug/L 96 11) 1,1-DICHLOROETHENE 8.03 61 1563675 38.83 ug/L 99 12) METHYLENE CHLORIDE 9.00 49 1633053 38.72 ug/L 99 13) METHYL TERT BUTYL ETHER 9.29 73 1466905 39.80 ug/L 99 14) TRANS-1,2-DICHLOROETHENE 9.65 61 1723088 42.79 ug/L 98 15) l,1-DICHLOROETHANE 10.54 63 2148117 41.59 ug/L 99 16) 2-BUTANONE (MEK) 11.36 43 271399 42.12 ug/L 99 17) 2,2-DICHLOROPROPANE 11.73 77 1900930 44.45 ug/L 98 18) CIS-1,2-DICHLOROETHENE 11.83 96 1176769 43.69 ug/L 95 19) CHLOROFORM 12.16 83 2116653 41.01 ug/L 100 20) BROMOCHLOROMETHANE 12.53 49 956257 39.28 ug/L 98 21) 1,2-DICHLOROETHANE 13.86 62 1320066 38.64 ug/L 99 24) 1,1,1-TRICHLOROETHANE 13.04 97 1782190 37.72 ug/L 100 25) l,l-DICHLOROPROPENE 13.38 75 1651538 39.37 ug/L 98 26) CARBON TETRACHLORIDE 13.62 117 1567629 37.98 ug/L 99 27) BENZENE 13.98 78 4679041 38.15 ug/L 99 28) TRICHLOROETHENE 15.24 95 1297493 40.15 ug/L 98 29) 1,2-DICHLOROPROPANE 15.58 63 1248220 37.19 ug/L 100 30) DIBROMOMETHANE 16.25 174 478714 39.91 ug/L 89 31) BROMODICHLOROMETHANE 16.09 83 1620303 37.44 ug/L 100 32) 2-CHLOROETHYL VINYL ETHER 16.59 63 407272 37.48 ug/L 95 33) Methyl iso-butyl ketone 16.65 58 203270 51.70 ug/L 98 ------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration 0110R40.D HP010402.M Fri Jan 11 09:02:21 2002 Page 1

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