WTC sample cover sheet, Dec 19 2001

NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed)

Data File : C:\HPCHEM\1\DATA\01dec24\1224C10A.D Vial: 9 Acq On : 24 Dec 2001 11:43 am Operator: 206-BH Sample : cal 10 Inst : GC/MS Ins Misc Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Time: Dec 24 12:22 2001 Quant Results File: HP121001.RES

Quant Method : C:\HPCHEM\1\METHODS\HP121001.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Last Update : Thu Dec 20 09:38:26 2001 Response via : Initial Calibration DataAcq Meth : HP121001

Compound R.T. Qlon Response Conc Unit Qvalue ------------------------------------------------------------------------- 34) CIS-1,3-DICHLOROPROPENE 17.18 75 549870 9.62 98 ug/L

35) TOLUENE 17.95 91 1524495 9.50 100 ug/L

36) TRANS-1,3-DICHLOROPROPENE 18.22 75 442462 9.97 ug/L 99 37) 1,1,2-TRICHLOROETHANE 18.60 97 211000 9.60 97 ug/L

38) TETRACHLOROETHENE 19.38 166 372974 9.85 98 ug/L

39) 1,3-DICHLOROPROPANE 19.12 76 409990 9.66 99 ug/L

40) DIBROMOCHLOROMETHANE 19.81 129 264847 9.91 ug/L 98 41) 1,2-DIBROMOETHANE 20.25 107 195910 9.36 95 ug/L

42) CHLOROBENZENE 21.13 112 1015091 9.51 98 ug/L

43-) 1,1,1,2-TETRACHLOROETHANE 21.17 131 351196 10.09 96 ug/L

44) 2-HEXANONE 18.51 43 121824 9.64 ug/L 98 45) ETHYLBENZENE 21.19 91 1973065 9.98 98 ug/L

46) P & M-XYLENE 21.34 106 1437038 19.35 99 ug/L

47) O-XYLENE 22.31 91 1620229 10.28 ug/L 100 48) STYRENE 22.38 104 1199410 9.79 ug/L 97 49) 1,1,2,2-TETRACHLOROETHANE 23.38 83 252553 10.74 100 ug/L

51) BROMOFORM 23.20 173 144608 9.02 99 ug/L

52) ISOPROPYLBENZENE 23.03 105 1943656 8.39 ug/L

99 53) 1,2,3-TRICHLOROPROPANE 23.71 110 68647 8.13 ug/L

96 54) N-PROPYLBENZENE 23.89 91 2580535 8.59 ug/L 100 55) BROMOBENZENE 24.13 156 428383 8.68 ug/L

90 56) 1,3,5-TRIMETHYLBENZENE 24.22 105 1664306 8.32 ug/L 100 57) 2-CHLOROTOLUENE 24.37 91 1557239 8.17 ug/L 96 58) 4-CHLOROTOLUENE 24.46 91 1594878 9.35 ug/L

97 59) TERT-BUTYLBENZENE 25.00 134 376927 8.82 ug/L 97 60) 1,2,4-TRIMETHYLBENZENE 25.10 105 1791720 8.63 ug/L 98 61) SEC-BUTYLBENZENE 25.46 105 2361191 8.47 ug/L

98 62) P-ISOPROPYLTOLUENE 25.72 119 1945739 8.70 ug/L

99 63) 1,3-DICHLOROBENZENE 26.08 146 969321 9.09 ug/L 98 64) 1,4-DICHLOROBENZENE 26.28 146 946983 8.87 ug/L 99 65) N-BUTYLBENZENE 26.60 91 2074166 9.69 ug/L

99 66) 1,2-DICHLOROBENZENE 27.13 146 813929 9.24 ug/L 98 67) 1,2-DIBROMO-3-CHLOROPROPAN 28.77 157 41729 9.27 ug/L 99 68) NITROBENZENE 28.97 77 370074 199.49 ug/L 97 69) 1,2,4-TRICHLOROBENZENE 30.71 180 460893 9.44 ug/L 99 70) HEXACHLOROBUTADIENE 30.96 225 265981 8.97 ug/L 99 71) NAPHTHALENE 31.39 128 507422 9.43 ug/L 99 72) 1,2,3-TRICHLOROBENZENE 31.94 180 340056 9.49 ug/L

99

------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration 1224C10A.D HP121001.M Mon Dec 24 12:22:23 2001 Page 2

NYC-WTC 000002412