Volatile organic compound analysis results, sample AD27764, Nov 2001

NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed) Data File : C:\HPCHEM\1\DATA\0lnovl5\1115C1OB.D Acq On Vial: 6 : 16 Nov 2001 1:42 am Operator: 206-BH Sample : cal 10 Inst : GC/MS Ins Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Time: Nov 16 2:20 2001 Quant Results File: HP110101.RES Quant Method : C:\HPCHEM\1\METHODS\HP110101.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Last Update : Fri Nov 02 15:17:46 2001 Response via : Initial Calibration DataAcq Meth : HP110101

Internal Standards R.T. Qlon Response Conc Units Dev(Min) 1) 1,4-DIFLUOROBENZENE 14.44 114 425636 5.00 ug/L 0.00 22) CHLOROBENZENE-D5 21.03 117 390231 5.00 ug/L 0.00 50) 1,4-DIFHUOROBENZENE-D4 26.18 152 196924 5.00 ug/L -0.02 System Monitoring Compounds 2) 1,2-DICHLOROETHANE-D4 13.65 65 162435 6.47 ug/L 0.00 Spiked Amount 5.000 Recovery = 129.40% 3) 4-BROMOFLUOROBENZENE 23.60 174 118824 5.37 ug/L 0.00 Spiked Amount 5.000 Recovery = 107.400 23) TOLUENE-D8 17.76 98 588404 4.99 ug/L 0.02 Spiked Amount 5.000 Recovery = 99.80% Target Compounds Qvalue 4) DICHLORODIFLUOROMETHANE 4.48 85 89362 7.86 ug/L 99 5) CHLOROMETHANE 4.99 50 132109 12.06 ug/L 99 6) VINYL CHLORIDE 5.17 62 112636 13.59 ug/L 98 7) BROMOMETHANE 6.08 94 101291 9.76 ug/L 96 8) CHLOROETHANE 6.20 64 82568 11.07 ug/L 94 9) TRICHLOROFLUOROMETHANE 6.74 101 190607 10.45 ug/L 99 10) ACETONE 7.68 43 33351 14.46 ug/L 98 11) 1,1-DICHLOROETHENE 8.02 61 312969 14.28 ug/L 89 12) METHYLENE CHLORIDE 9.00 49 347417 14.52 ug/L 89 13) METHYL TERT BUTYL ETHER 9.29 73 333865 8.22 ug/L 97 14) TRANS-1,2-DICHLOROETHENE 9.65 61 353757 14.39 ug/L 91 15) 1,1-DICHLOROETHANE 10.52 63 436841 13.57 ug/L 99 16) 2-BUTANONE (MEK) 11.35 43 54766 11.72 ug/L 93 17) 2,2-DICHLOROPROPANE 11.73 77 277418 11.47 ug/L 94 18) CIS-1,2-DICHLOROETHENE 11.81 96 209519 12.09 ug/L 81 19) CHLOROFORM 12.14 83 389894 13.56 ug/L 99 20) BROMOCHLOROMETHANE 12.51 49 210780 14.65 ug/L 81 21) 1,2-DICHLOROETHANE 13.84 62 270710 15.42 ug/L 97 24) 1,1,1-TRICHLOROETHANE 13.04 97 308983 13.31 ug/L 99 25) 1,1-DICHLOROPROPENE 13.36 75 309691 12.20 ug/L 94 26) CARBON TETRACHLORIDE 13.62 117 233586 13.08 ug/L 98 27) BENZENE 13.96 78 959922 12.09 ug/L 100 28) TRICHLOROETHENE 15.22 95 217312 11.66 ug/L 93 29) 1,2-DICHLOROPROPANE 15.58 63 270486 12.89 ug/L 98 30) DIBROMOMETHANE 16.23 174 53013 10.46 ug/L 75 31) BROMODICHLOROMETHANE 16.07 83 273935 13.04 ug/L 100 32) 2-CHLOROETHYL VINYL ETHER 16.57 63 75122 12.63 ug/L 94 33) Methyl iso-butyl ketone 16.65 58 42337 13.23 ug/L 76 ------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration 1115C10B.D HP110101.M Fri Nov 16 02:20:51 2001 Page 1

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