Volatile organic compound analysis results, sample AD27764, Nov 2001

NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed) Data File : C:\HPCHEM\1\DATA\O1NOV16\1116C10.D Vial: 6 Acq On : 16 Nov 2001 9:52 am Operator: 206-BH Sample : cal 10 Inst : GC/MS Ins Misc Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Time: Nov 16 10:31 2001 Quant Results File: HP110101.RES

Quant Method : C:\HPCHEM\l\METHODS\HP110101.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Last Update : Fri Nov 02 15:17:46 2001 Response via : Initial Calibration DataAcq Meth : HP110101

Internal Standards R.T. Qlon Response Conc Units Dev(Min)

1) 1,4-DIFLUOROBENZENE 14.42 114 577985 5.00 ug/L -0.02 22) CHLOROBENZENE-D5 21.01 117 482015 5.00 ug/L -0.02 50) 1,4-DICHLOROBENZENE-D4 26.18 152 273662 5.00 ug/L -0.02 System Monitoring Compounds 2) 1,2-DICHLOROETHANE-D4 13.64 65 199928 5.86 ug/L -0.02 Spiked Amount 5.000 Recovery = 117.20% 3) 4-BROMOFLUOROBENZENE 23.59 174 167543 5.58 ug/L -0.02 Spiked Amount 5.000 Recovery = 111.600 23) TOLUENE-D8 17.74 98 716463 4.92 ug/L 0.00 Spiked Amount 5.000 Recovery = 98.400

Target Compounds Qvalue 4) DICHLORODIFLUOROMETHANE 4.48 85 292939 18.97 ug/L 98 5) CHLOROMETHANE 4.98 50 196911 13.23 ug/L 98 6) VINYL CHLORIDE 5.15 62 181836 16.15 ug/L 98 7) BROMOMETHANE 6.06 94 177270 12.58 ug/L 98 8) CHLOROETHANE 6.20 64 130819 12.92 ug/L 96 9) TRICHLOROFLUOROMETHANE 6.74 101 398218 16.08 ug/L 99 10) ACETONE 7.66 43 37510 11.98 ug/L 96 11) l,1-DICHLOROETHENE 8.02 61 411232 13.81 ug/L 95 12) METHYLENE CHLORIDE 8.99 49 402219 12.38 ug/L 94 13) METHYL TERT BUTYL ETHER 9.28 73 429316 7.79 ug/L 96 14) TRANS-1,2-DICHLOROETHENE 9.63 61 425714 12.75 ug/L 96 15) 1,1-DICHLOROETHANE 10.52 63 542146 12.40 ug/L 99 16) 2-BUTANONE (MEK) 11.34 43 64153 10.11 ug/L 96 17) 2,2-DICHLOROPROPANE 11.71 77 438822 13.36 ug/L 97 18) CIS-1,2-DICHLOROETHENE 11.80 96 263993 11.22 ug/L 87 19) CHLOROFORM 12.14 83 490282 12.56 ug/L 99 20) BROMOCHLOROMETHANE 12.51 49 243208 12.45 ug/L 96 21) 1,2-DICHLOROETHANE 13.84 62 320816 13.46 ug/L 98 24) 1,1,1-TRICHLOROETHANE 13.02 97 404460 14.10 ug/L 99 25) 1,1-DICHLOROPROPENE 13.37 75 387218 12.35 ug/L 100 26) CARBON TETRACHLORIDE 13.60 117 319831 14.50 ug/L 99 27) BENZENE 13.94 78 1117232 11.39 ug/L 100 28) TRICHLOROETHENE 15.22 95 272111 11.82 ug/L 99 29) 1,2-DICHLOROPROPANE 15.56 63 309076 11.92 ug/L 100 30) DIBROMOMETHANE 16.21 174 75919 12.13 ug/L 85 31) BROMODICHLOROMETHANE 16.06 83 337658 13.01 ug/L 99 32) 2-CHLOROETHYL VINYL ETHER 16.57 63 89027 12.11 ug/L 98 33) Methyl iso-butyl ketone 16.64 58 47041 11.90 ug/L 79 ------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration 1116C10.D HP110101.M Fri Nov 16 14:09:10 2001 Page 1

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