NYC-WTC_000209823

NYC 9/11 Public Portal Document

Mov 01 01 01:12p PSC Rnalytical Services G103219B67 P.5 OCT 25 2001 5:02 PM PR PHILP fiNALVL1CAL9B5 332 9169 TO 16109219667 P.03>'04

PigeJ of* 10/26rt001 - PASC- Certificate ofAnalysis

207720 207720 207720 207720 207720 1467964 1467961 1467962 1467963 f/illipRfaanglD: 1457960 062401 01 06240201 062403 01 062404 01 062400 01 07-01 D5-O2 05-03 D6-O2 aieniJO D6-01 13-Oct-2001 13-0ct-2001 13.0ct-200l 13-OCI-2Q01 13.0cl-2001 Hate SeiKpledt Component MOL Caits 11000 24000 14000 12000 Totil TttracWorodlbenzofuracs pe/s 1500 6700 15000 S800 5000 T«ul PeuUdtlorodibenioftirans 610 3500 7900 4000 1900 Total Hexichlorodibciuofutsjis 230 730 1200 630 450 Total HepiaeWorotlibiiizoftifans 62 460 91 1100 1100 430 Ocaehlorodibenzofuran ZIOOO 11000 14000 1000 13000 Total TclrlchlOrtidibejUO-p-diOXiP9 2800 3100 4100 190 4600 Total Pentachlocodibenzop-dloxins 4700 2400 2700 280 3900 Total H«achlorodibenzo-p-<Jloxln$ 1600 950 920 190 1400 Total Heptichlorodibcnzo-p-dtoxina 2000 1400 2300 1100 3400 Oetaehlorodibenzo-p-dioxin Internal Recoverits % 62 62 54 57 42 2,3,7.g-T4CDF-13C12 44 65 68 2.3.7.8.T4CDD-13C12 58 63 55 66 40 57 59 l,2p,7,5-P5CDF-I3C12 65 79 82 1,2,3.7.8.P5CDD.13C12 122 97 47 62 40 59 58 1,2,3,4,7,8-H6CDF-13CI2 63 64 46 68 43 1,2,3,6,7,8-H6CDI>-13C12 44 68 69 1 ;t;3.4,6.7,«-H7CDF-l 3C12 48 71 85 47 76 77 1,23,4.6,7,8-H7CDD-13CI2 73 75 52 79 80 OCDD-l3Ct2 54

170 1200 2400 1300 1400 2.3,7.8-a4-DibenzoHjran (DBS) pg/g 29 27 3.9 33 61 2|3 (7,8-Cl 4 -D iben np-p-diox* n 250 ISO 33 230 490 l,2,3.7,8-CI5-Dibatzofur8n 540 310 48 380 930 2,3,4,7,8-CI5-Dibcnzofutan <49 <40 <3.5 <52 <97 l,2,3.7,!-€15-Diben2o-p-dioxin 510 340 46 530 1000 l,2,3,4,7,&-a6-DibeMOforan ISO <26 230 470 2W l,2,3,6,7.8-Cl6-DibeMofwan ISO <40 250 370 230 2,3.4.6.7.8-a6-Qibenzofuran <53 <3.3 <74 150 50 1.2.3,7,«.9-Cl6-Dtbtni.ofutan <6.7 68 76 38 38 1,2,3,4,7,8-C16-Dibenzo-p-6ioxtn 75 1,23,6,7,8-a6-Dibenzo-p-dioxin <10 no 130 66 <7.7 140 210 120 120 I,2,3,7.8,9-a6-Dibenzo-i>-dioxin <450 1.2,3.4.6,7.a-C17-Dibnuofuun <83 <870 <1300 <820 <5.1 300 560 240 130 1,2.3.4.7,8.9-C17-Dibert2orutan 440 98 710 750 420 l,2,3,4,6,7,8-C17-Dibcrao-p-dioxin 460 91 1100 1100 630 t,2,3,4,6,7,8,9-ClS-Dibtnzc!futan 2300 1100 3400 2000 1400 1.2.3,4,6.7,8,9-a3-Dlben2o-p-<Iioxm 10 10 DiluHon Factor 10 10 10

26 130 570 ISO 200 2,3.7,8-TCDF (DB225) pe/g InlemiRReeovaies % 60 68 47 75 74 2,3,7,8.TCDF-13C12

Client:Philip Analyticd Sorvieos Inc Project:Misc.

CITY_DEP_WORBY_CANNATA_SUBP_000002143

NYC-WTC_000209824