ATC ASSOCIATES INC. TEM ANALYSIS
LAB GROUP # 10/13/01
Lab Sample No. 61642 Filter Type MCE 2E mm Operator
Client; Spl. Nc. 10 Filter Area 38E mm
Instrument I.D. EM IC CRX Grid I-D. 5^^ A/ Disk No.
Screen Magnification 16,400X (GO’ Area 0.01124 mm"2 Comments
Acc. Voltage 80 kV Nc. GO to be Analyzed _4 3.14'7 Struct. Corspd. no TO 5/mm"2.)
GO. Structure Structure Type Length I.D. of Structure EDS
N or
^0.5 um
(Nonasb.
No Coord. No. F B C M > Sum Chrys. Amphibole Nonasb. Ambig./ND Elements)
< 5 um
/
'I
5
IL /r
Photo No. (from 1 in 5 asbeatoa— identify all atructurea uaing EPS Check diffraction for asbeatoa Store all unrepeated apectra—
containing samples) Grid acceptance:! atructurea up to 70s/&ni (l»t 4)
<50% undiaaolved filter, overlapped or folded
Struct, s > 0.5um & > 5:1 Aspect Ratio
N= Not Observed (EDS spectrum or diffrsction pattern)
<10% particulate coverage >50% coverage
at least 20 unfolded or overlapped grid squares
Totals
Positive diffraction pattern properties conforming <5% holes or opaque areas F B C M > 5um
to laboratory idenUfication criteria observed. •Unuked portion
Par chrykolllB: 0.7anm spacing for (020) rwriectlona. of filter
Chrysotile
Q.53nm spacing for the layer line repeal, streaking .voided portion
of (110) and (130) reflecUons. of filler
Por amphiboles: O.S3nm layer Une repeat, and approx. Portion of filter (Smm wide)
3.5 ratio of nen-lwinned layer line spot apaeing to •ubject to
examination
Amphibole
layer line repeal distance (Q.Mnm).
EDS spectrum conforming to laboratory
identification criteria observed. AMPHIBOLES Ambiguous
P= Single Fiber (1-3 interaectiona = 1—3 fibers) Amosite
0= Bundle (>3 fibers <1 fiber diameter apart)
C= Cluster (>3 Intersections)
SSmni filter Crocidolite Non—asbestos
J stopping Rules; I--------- - Anthophyllite
M- Matrix
NSD= Nq Structures Detected
L:\DATA\PRlVATr\MlKEC\ CADOXTEMO
[
>50 »/C.O. or tn lat 4 G.O.
B/22/«a
Tremolite
Actinolite Non-Identified
CITY_21MC100_003082337
NYC-WTC_000188668
OCR can misread numbers and units. Confirm readings against the page image before using them.
NYC-WTC_000188668Source: NYC Law Department, mirrored locally
Laboratory report containing transmission electron microscopy data and images for asbestos fiber identification from samples analyzed in September 2001.