PCDD/PCDF analysis results, Jan 2002

NYC 9/11 Public Portal Document

Page No. 3 Listing of S020235B.dbf 01/17/2002 Matched GC Peaks / Ratio / Ret. Time

“Ound/ .. QC.Log Omit Why ..RT. OK Ratio Total.Area/Ht Area/Ht Peakl Area/Ht.Peak2 Rel.RT Compound.Name.. ID. Flags.

X X 31:56 RO 1.83 2 9 7- 21.32 11.67 1.045 J 32:12 1 . 58 114. C‘b 69.86 44.22 1.053 DC 3 2:26 1 . 65 18.15 1.061 340-342 16 Peaks 12.626.14

13C12-PeCDF 1.32-1.78 0.869-1.131 352-354 DC NL Height I 0,74 0.55 0.19 29:26 RO1 4.09 2.98 4.79 1.17 0.963 30:34 1.44 2,840.71 1.676.30 1,164.41 1.000 13C12-PeCDF 123 IS2 Height 885.91 525.95 359.96 30:50 RO► 0.42 15.05 9.15 31. 80 1.009 31:14 1, 46 2,703.72 1,613.72 1,090.00 1.022 13C12-PeCDF 234 SURI 32:11 RO• 0.78 26.47 16.09 2 0.57 1.053 352-354 5 Peaks 5,586.93

Above: PeCDP / PeCDD Follows

PeCDD 1.32-1.78 0.940-1.021 356-358 DC NL Height 0.77 0.46 0.31 2 9:50 1.58 B.013.57 4,911.06 3.1C2.51 0.946 3 0:18 1.51 308.94 185,74 123.20 0-960 30:31 1.55 3.439.21 2,089.34 1.349,87 0.967 30:40 1.35 313.41 180.31 133.10 0.972 30:51 1.54 2.285.30 1.385,59 099.71 0.978 31:05 1.50 655.90 393.31 262.59 0.965 31:17 1.55 1.670.95 1,016.70 654.25 0.992 31:25 RO 0.99 449.43 273.18 275.47 0.996 M 31:34 RO 1.04 227.03 136.00 133.00 1.001 12378-PeCDD AN 31:42 RO 1.19 203.02 95.44 79.93 1.005 32:02 RO 0.99 152.33 92.59 93.30 1.015 J6-358 11 Peaks 17,719.89

13C12-P€CDD 1.32-1.78 0.873-1.127 368-370 DC NL Height 0.30 0.21 0.09 30:31 1.72 3 .76 2.38 1.38 0.967 30:50 RO) 0.50 2.27 1.38 2.74 0.977 31:33 1.4S 1,770.00 1,056.57 713.43 1.000 13C12-PeCDD 123 IS3 Height 555.95 351.03 234.92 32:16 RO) 0,87 7.29 4.43 5.07 1.023 360-370 4 Peaks 1,783.32

Above: PeCDD / HxCDF Follows

HxCDF 1.05-1.43 0.964-1.045 374-376 DC NL Height 2.76 1.22 1,54 33:00 1.25 157.36 87.49 69.87 0.970 33:08 1.27 635.76 355.5S 280.IS 0,974 33:18 1.27 42.58 23.79 16.79 0,978 33:25 1.25 124.07 69.03 55.04 0,982 33:34 1.27 133.00 '■4 76 59.04 0.986 33:56 1.24 1,083.11 699 50 483.61 0.997 133479-HxCDF AN 34:03 1,24 361.90 ZOO.21 161.59 1.000 123678-HxCDF AN

Triangle Laboratories, Inc.® 801 Capitola Drive • Durham, North Carolina 27713 Printed: 13:46 01/17/2002 Phone: (919) 544-5729 • Fax: (919) 544-5491 153

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