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114 Liberty PAH analytical results validation documentation, March 2003

Machine-extracted title · confidence 80%

EPA request for verification documentation of revised PAH analysis methodology at 114 Liberty, noting analytical date discrepancies.

NYC-WTC_000155360–000155393

Folder label: “114 LIBERTY 2 OF 2”

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NYC 9/11 Public Portal Document

PSC AWOWAL INDUSTRIAL HYGIENE ENVIRONMENTAL TESTING SEWICES .EPAPA-00136 •AIHA ACCREDITATION NO. 100439 *MYDOH/NELAC 10903 ’PA DEP 06-353 •N3DBPPA020 •CT DPH PH-0238 UIS Pottsville Pike Reading, PA 196BS .NCDHSR599 (Tel) 618<921>8833 fax) S18-921-9687 Date: 24-Mar-03

CLIENT: JLC Env. Consultants Inc. Lab Order: R03030157 Project: US DEP WTC - LBA (Dioxin & PAH wipes)

Lab ID: R03030157-13 Collection Date: 3/5/2003 Client Sample ID: 04,9th Fir (Floor Hallway) Matrix: WIPE Analyses Result Limit Qual Units DF Date Analyzed

POLY AROMATIC HYDROCARBONS SW8270C Analyst: CXA Acenaphthene BRL 1.0 pg. Total 1 3/10/200311:15:00 PM Acenaphthylene BRL 1.0 pg, Total 1 3/10/2003 11:15:00 PM Anthracene BRL 1.0 pg. Total 1 3/10/2003 11:15:00 PM Benzo(a)anthracene BRL 1.0 pg. Total 1 3/10/2003 11:15:00 PM Benzo(a)pyrene BRL 1.0 pg. Total 1 3/10/2003 11:15:00 PM Benzo(b)fluoranthene BRL 1.0 pg. Total 1 3/10/2003 11:15:00 PM Benzo(g.h.i)perylene BRL 1.0 pg. Total 1 3/10/2003 11:15:00 PM Benzo(k)fluoranthene BRL 1.0 pg. Total 1 3/10/2003 11:15:00 PM Chrysene BRL 1.0 pg. Total 1 3/10/200311:15:00 PM Dibenzo(a.h)anthracene BRL 1.0 pg. Total 1 3/10/2003 11:15:00 PM Fluoranthene BRL 1.0 pg. Total 1 3/10/200311:15:00 PM Fluorene BRL 1.0 pg. Total 1 3/10/2003 11:15:00 PM lndeno(1.2.3-cd)pyrene BRL 1.0 pg, Total 1 3/10/2003 11:15:00 PM Naphthalene BRL 1.0 pg. Total 1 3/10/2003 11:15:00 PM Phenanthrene BRL 1.0 pg. Total 1 3/10/2003 11:15:00 PM Pyrene BRL 1.0 pg. Total 1 3/10/2003 11:15:00 PM

Qualiflers: BRL - Below Reporting Limit S - Spike Recovery outside accepted recovery limits J - Analyte detected below quantitation limits R - RPD outside accepted recovery limits B - Analyte detected in the associated Method Blank E - Value above quantitation range * - Value exceeds Maximum Contaminant Level Page 13 of 15

NYC-WTC_000155375

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NYC-WTC_000155375Source: NYC Law Department, mirrored locally

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