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114 Liberty PAH analytical results validation documentation, March 2003

Machine-extracted title · confidence 80%

EPA request for verification documentation of revised PAH analysis methodology at 114 Liberty, noting analytical date discrepancies.

NYC-WTC_000155360–000155393

Folder label: “114 LIBERTY 2 OF 2

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NYC 9/11 Public Portal Document

PSC AWALVneAL INDUSTRIAL HYGIENE ENVIRONMENTAL TESTING

SERVICES •EPA PA-00136 •AIHA ACCREDITATION NO. 100439 ’NY DOH/NHAC10908 ‘PA OB’ Ofr-353 •NJDS>PM)20 •CT DPH PH-0238 *418 Pottsville Pike Reading, PA 136BS •NCDENR599 (Tel) 810-921-8833 (Fax) 818-921-9887 Date: 24-Mar-03

CLIENT: JLC Env. Consultants Inc. Lab Order: R03030157 Project: US DEP WTC - LBA (Dioxin & PAH wipes)

Lab ID: R03030157-10 Collection Date: 3/5/2003 Client Sample ID: 04,7th Fir (Floor Hallway) Matrix: WIPE Analyses Result Limit Qual Units DF Date Analyzed

POLY AROMATIC HYDROCARBONS SW8270C Analyst: CXA Acenaphthene BRL 1.0 pg, Total 1 3/10/2003 10:01:00 PM Acenaphthylene BRL 1.0 pg, Total 1 3/10/2003 10:01:00 PM Anthracene BRL 1.0 pg. Total 1 3/10/2003 10:01:00 PM Benzo(a)anthracene BRL 1.0 pg, Total 1 3/10/2003 10:01:00 PM Benzo(a)pyrene BRL 1.0 pg. Total 1 3/10/2003 10:01:00 PM Benzo(b)fluoranthene BRL 1.0 pg. Total 1 3/10/2003 10:01:00 PM Benzo(g,h.i)perylene BRL 1.0 pg, Total 1 3/10/2003 10:01:00 PM B8nzo(k)fluotanthene BRL 1.0 pg. Total 1 3/10/2003 10:01:00 PM Chrysene BRL 1.0 pg. Total 1 3/10/2003 10:01:00 PM Dibenzo(a.h)anthracene BRL 1.0 pg. Total 1 3/10/2003 10:01:00 PM Fluoranthene BRL 1.0 pg. Total 1 3/10/2003 10:01:00 PM Fluorene BRL 1.0 pg. Total 1 3/10/2003 10:01:00 PM lndeno(1.2.3-cd)pyrene BRL 1.0 pg. Total 1 3/10/2003 10:01:00 PM Naphthalene BRL 1.0 pg. Total 1 3/10/2003 10:01:00 PM Phenanthrene BRL 1.0 pg. Total 1 3/10/2003 10:01:00 PM Pyrene BRL 1.0 pg, Total 1 3/10/2003 10:01:00 PM

Qualifiers: BRL - Below Reporting Limit S - Spike Recovery outside accepted recovery limits J - Analyte detected below quantitation limits R - RPD outside accepted recovery limits B - Analyte detected in the associated Method Blank E - Value above quantitation range ♦ - Value exceeds Maximum Contaminant Level Page 10 of 15

NYC-WTC_000155372

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NYC-WTC_000155372Source: NYC Law Department, mirrored locally

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