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114 Liberty PAH analytical results validation documentation, March 2003

Machine-extracted title · confidence 80%

EPA request for verification documentation of revised PAH analysis methodology at 114 Liberty, noting analytical date discrepancies.

NYC-WTC_000155360–000155393

Folder label: “114 LIBERTY 2 OF 2

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NYC 9/11 Public Portal Document

INDUSTRIAL HYGIENE ENVIRONMENTAL TESTING PSC «>A PA-00136 •NY OOH/NQAC10908 •NJDH’PAOZO •AIHA ZWCREDITATION NO. 100439 •PA DEP 06-353 •CT DPH PH-0238 441S Pottsville Pike Reading, PA 1S8BS •NCDBSRS99 (Tel) 610*SSt<»33 (Fax) S1B-921.9JB7 Date: 24-Mar-03

CLIENT: JLC Env. Consultants Inc. Lab Order: R03030157 Project: US DEP WTC - LBA (Dioxin & PAH wipes)

Lab ID: R03030157-08 Collection Date: 3/4/2003 Client Sample ID: 05, 10th Fir (Wall Kitchen) Matrix: WIPE Analyses Result Limit Qual Units DF Date Analyzed

POLY AROMATIC HYDROCARBONS SW8270C Analyst: CXA Acenaphthene BRL 1.0 pg, Total 1 3/10/2003 9:12:00 PM Acenaphthylene BRL 1.0 pg, Total 1 3/10/2003 9:12:00 PM Anthracene BRL 1.0 pg. Total 1 3/10/2003 9:12:00 PM Benzo(a)anthracene BRL 1.0 pg. Total 1 3/10/2003 9:12:00 PM Benzo(a)pyrene BRL 1.0 pg. Total 1 3/10/2003 9:12:00 PM Benzo(b)fluoranthene BRL 1.0 pg, Total 1 3/10/2003 9:12:00 PM Benzo(g,h,i)perylene BRL 1.0 pg, Total 1 3/10^003 9:12:00 PM Benzo(k)fluoranthene BRL 1.0 pg. Total 1 3/10/2003 9:12:00 PM Chrysene BRL 1.0 pg. Total 1 3/10/2003 9:12:00 PM Dibenzo(a,h)anthracene BRL 1.0 pg. Total 1 3/10/2003 9:12:00 PM Fluoranthene BRL 1.0 pg. Total 1 3/10/2003 9:12:00 PM Fluorene BRL 1.0 pg, Total 1 3/10/2003 9:12:00 PM lndeno(1,2,3-cd)pyrene BRL 1.0 pg, Total 1 3/10/2003 9:12:00 PM Naphthalene BRL 1.0 pg. Total 1 3/10/2003 9:12:00 PM Phenanthrene BRL 1.0 pg. Total 1 3/10/2003 9:12:00 PM Pyrene BRL 1.0 pg. Total 1 3/10/2003 9:12:00 PM

Qualifiers: BRL-Below Repotting Limit S - Spike Recoveiy outside accepted recovery limits J - Analyte detected below quantitation limits R - RPD outside accepted recovery limits B - Analyte detected in the associated Method Blank E - Value above quantitation range * - Value exceeds Maximum Contaminant Level Page 8 of 15

NYC-WTC_000155370

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NYC-WTC_000155370Source: NYC Law Department, mirrored locally

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