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Document / 271 pages

Chain of custody form, 90 Church Street, Nov 2001

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Chain of custody document for samples from 90 Church Street dated November 14, 2001.

NYC-WTC_000124631–000124901

Folder label: “74-90 CHURCH ST 1001230, 86/1

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NYC 9/11 Public Portal Document

CASE NARRATIVE

STL SACRAMENTO PROJECT NUMBER GIJ270136

SOLID, 8290, Dioxins/Furans The total TCDD result for sample D-8-04 comes from a lOX dilution since it saturated the instrument detector on the 1X dilution.

WIPE, 8290, Dioxins/Furans The 1,2,3,4,6,7,8-HpCDF result in sample D-6-07 has been flagged with a `JA' qualifier due to a matrix interference that caused the ion ratios to be outside limits. The analyst believes the analyse to be present, but the quantitation is estimated since it is based on theoretical ratios. Sample D-6-07 shows a matrix related interference that causes the suppression of several peaks. The sample was analyzed at a dilution on another instrument and the original results were confirmed. The internal standard recoveries for 13C-OCDD & 13C-1,2,3,4,7,8- HxCDF are outside control limits. The results for 1,2,3,6,7,8-HxCDF, 2,3,4,6,7,8-HxCDF, total HxCDF, & total HpCDD may be biased low. The results for l,2,3,4,7,8-HxCDD, l,2,3,7,8,9-HxCDD, total HxCDD, 1,2,3,4,7,8,9-HpCDF, & total HpCDF maybe biased • high

There were no other anomalies associated with this project.

G1J270136 STL - Sacramento (918)373-5600 lot 51 NYC-WTC 000124847

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NYC-WTC_000124847Source: NYC Law Department, mirrored locally

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