NYC 9/11 Public Portal Document
02/20/2002 09:03 FAX Q 021
.,.,, . JLC ENV RONMEHTPL N0.8n P.IR
Maze Croup LI.0 (104 John Street)
JLC Project # C1,2D94aOf pagre 2
I'ntruductfon
Pdarlzed light dispersion Is the
asbestos In bulk method far
s. it s n t
method {JLC lab d~rgbulkdi tori'alanalyses.
MethQdasbrgy
A ctain of custody is kept for each sanpIe to ensure proper handling
awtysts. To avoid any possible eontemtrtotlon, all same and slide and delivery to the JLC tab prior to
ventpa HEPA-filter hood with corrtirnOu8 airflow. Sample anaemiapreparation
Is perbrmed
is carried out in a
using PLM-DS In
accordance with the USEPA ,'Method for is DstemiInatlon of Asbestos In
EPA S00 8.83115, July 1983, and NiYQQH-EI.AP certlPic atIon Sulk Su€tdng Mataadals,"
manual,
Methods for ld#sntifylnp and tuarstitating Asbestos in Bulk $samples," "Polarized Light Microscope
ELAP 198.1, October 1993.
ern&ytic i Procedtsms •
All sanpies are subject to preliminary visual stememlcroscopc
,AN id camiria#fon. Observation of homogeneity,
cation, and semiqusntltation of c nst3tusnts can be triads
at this point Samples lacdng
uniformity of composition endlnr distribution of component rnats,fals then undergo
non-friable organically bound (NOB) fi les such as floor tiles and hcmogeniz tion. Some
steps to dislodge problem matrices O,e. ashina. +e*ractians, and TLM). roofing matertais may require additional
ldantiflcatJan of suspect fibers in made by PIJM analysis of subsamples.
polarising flitera enables cis to observe speciltc opti i oh otedatkos A mic mscape equipped With dual
of asbestos requires d termination of the foU lraQ of esdt sample. Positive Identification
opeal propertias;
rsfracflvs lockers, birefringerice, axdndion rJ,eracwleljcs, end morphology, color and pieochroiam,
signs of 6iorlgs floe.
~, Asbestos quen Caron is performed by point-counting procedctrs►
dearmin the reiadve areas ocr upland by separate minerals a standard technique in petrography for
or points Aver the micrceoope-s field of view. Then bar of inants rack. An ocular reticle superimposes
mimes a point
pa~ras ~ fiber Is neaordaat. A total of 400 Pants must fro positioned thready above each kind of
~ be counted over at heat eight different representative
subsarlor to r~rr►pit% analysis.
Polasrasd Ught Mlarasoapy
JLC uses an Wyrnpus l3HT.p Polarizing Mi
scapccrnpiae with polarizer, analyzer, port for wave
r tardatten plat 380 9i rot rQ stage, stage condenser, lamp end lamp i~a$, eyepiece
ratio degree Roint you t fight aaailowaa for the determination of refraction
indices relative to sp '
c cremations, Morphology and color can also be observed
plane polarized fight Obssrvatien of particles or fibers under
while oriented between polarletng filters whose
privileged vibrrnton directions are perpendIc r allows
exanctlon dxracteriaifics of snisatroplc paartideg, 5n4 for dets> m inon of isotroplsmt aanis'COplsm,
be placed in the polarized light paste for verification maculation of bireftingarns'. A retardation plate may
of signs of Notation.
Ma lytegi Results
The "Summery Of Analytical Results* rapr*santa the
results of analysis, Positive results mean die sample
is aaabeatc or contains more than one percent asbestos
ldintlfl tj and quantftetiorl of major ooncentre1Jc a Of by weight The rsaujts are generally suPtdent for
atdIt onai techniques may be necessary. Pisses b8 aware autos, However,, It may be found that
that PLM is not aonslsterdy reeable in
detecting asbeatca in floor coverings and simnilar NOD materials,
trued as wort.asbestos containing. confirmation must be maw Def rs ttla material can os considered or
Microscopy (TEM), by quantitative TransmIston 81ectrcn
2f
NYC-WTC 000123818
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