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Document / 7 pages

Pesticide CCV results, sample AD26335, Nov-Dec 2001

Machine-extracted title · confidence 95%

Calibration verification report for pesticide analysis of sample AD26335 showing recovery percentages for standard compounds.

NYC-WTC_000092387–000092393

Folder label: “508 X 11/5/01 A 12/1/01

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Scanned page image, NYC-WTC_000092388
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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Signal #1 : C:\MSDCHEM\1\DATA\5O8\O112O1\3PESTC2.D\ECD1A.CH Vial: 72 Signal #2 : C:\MSDCHEM\1\DATA\508\011201\3 PESTC2.D\ECD2 B.CH Acq On : 04 Dec 2001 10:08 am Operator: Nefliu Sample : pest ccv2 Inst : Instrume Mise : Multiplr: 1.00 IntFile Signal #1: EVENTS.E IntFile Signal #2: events2.e Quant Time: Dec 12 11:19:16 2001 Quant Results File: 011203P.RES

Quant Method : C:\MSDCHEM\l\METHODS\dll203P.M (Chemstation Integrator) Title : 508 Chlorinated Pesticides Last Update : Mon Dec 03 10:48:55 2001 Response via : Initial Calibration DataAcq Meth : 508.M

Volume Inj. Signal #1 Phase Signal #2 Phase: Signal #1 Info Signal #2 Info : Compound RT#1 RT#2 Resp#l Resp#2 ug/1 ug/1

System Monitoring Compounds 10) s 2,4-DDD SURROGAT 14.47 15.05 573.4E6 517.2E6 0.202m 0.205 Spiked Amount 0.200 Recovery = 101.00% 102.50% Target Compounds 1) Propachlor 9.18 8.60 85836884 66753127 0.202 |/)|y. 0.207 2) g-BHC 9.96 10.27 1971.7E6 1728.0E6 0.300 0.301 3) Heptachlor 11.12 11.32 571.7E6 434.9E6 0.102 ,^,{,4 0.107 4) Aldrin 11.83 12.06 774.3E6 711.9E6 0.125 0.125 5) Heptachlor Epoxi 13.26 13.41 1372.1E6 1243.2E6 0.251 (orf 0.248 6) 4,4-DDE 14.09 14.62 2135.8E6 1993.7E6 0.414 1047. 0.411 7) Dieldrin 14.67 14.88 451.1E6 417.3E6 0 . OSOm^oO'/- 0.084 8) Endrin 15.18 15.54 749.6E6 752.7E6 0.216rri |«<f.0.216 9) Methoxychlor 17.12 18.08 715.2E6 525.1E6 0.392m«jf(. 0.384

(f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int. 3PESTC2.D 011203P.M Wed Dec 12 11:20:10 2001 Page 1

NYC-WTC_000092388

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NYC-WTC_000092388Source: NYC Law Department, mirrored locally

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