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← Document results/DEP Box 68/508 X 11/2/01 A 11/30/01
Document / 6 pages

Pesticide chromatogram review, Dec 2001

Machine-extracted title · confidence 100%

Review of chromatographic data for pesticide analysis including signal peaks and recovery calculations.

NYC-WTC_000091905–000091910

Folder label: “508 X 11/2/01 A 11/30/01

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Scanned page image, NYC-WTC_000091909
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Signal #1 C:\HPCHEM\l\DATA\508\113001\PRL1016.D\ECDlA.CH Vial: 51 Signal #2 C:\HPCHEM\l\DATA\508\113001\PRL1016.D\ECD2B.CH Acq On 1 Dec 2001 10:17 pm Operator: Nefliu Sample prllOie Inst 105 Mise : Multiplr: 1.00 IntFile Signal #1: events.e IntFile Signal #2: events2.e Quant Time: Dec 10 15:29 2001 Quant Results File: PCB1016.RES

Quant Method : C:\HPCHEM\1\METHODS\508\PCB1016.M (Chemstation Integrator) Title : Arochlor 1016 Last Update : Mon Dec 10 15:18:09 2001 Response via : Initial Calibration DataAcq Meth : PESTPCB.M

Volume Inj. Signal #1 Phase Signal #2 Phase: Signal #1 Info Signal #2 Info :

Compound RT#1 RT#2 Resp#l Resp#2 ug/1 ug/1

System Monitoring Compounds 7) s 2,4-DDD Surrogat 21.62 21.91 3236612 225298 0.132m 0.145 Spiked Amount 0.200 Recovery •' = 66.00% 72.50%

Target Compounds 1) 1016-1 14.40 14.88 151393 9504 0.135m 0.132m 2) 1016-2 15.54 16.16 290614 24325 0.134 0.128 3) 1016-3 16.87 17.02 602880 6747 0.155m 0.135 4) 1016-4 17.51 17.70 243692 8872 0.238m 0.147m# 5) 1016-5 17.83 18.11 423513 25145 0.179 0.270m# 6) 1016-6 18.69 19.03 159287 11021 0.140m 0.164m

(f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int. PRL1016.D PCB1016.M Mon Dec 10 15:29:47 2001 Page 1

NYC-WTC_000091909

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NYC-WTC_000091909Source: NYC Law Department, mirrored locally

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