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← Document results/DEP Box 68/508 X 11/7/01 A 12/1/01
Document / 11 pages

Pesticide calibration verification results, sample AD26538, Nov-Dec 2001

Machine-extracted title · confidence 90%

Laboratory report showing recovery percentages for pesticides and PCBs in sample AD26538 analyzed between November and December 2001.

NYC-WTC_000091283–000091293

Folder label: “508 X 11/7/01 A 12/1/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Signal #1 C:\HPCHEM\l\DATA\508105\113001\2PESTC2.D\ECDlA.CH Vial: 52 Signal #2 C:\HPCHEM\l\DATA\508105\113001\2PESTC2.D\ECD2B.CH Acq On 1 Dec 2001 10:55 pm Operator: Nefliu Sample pestccvl Inst : 105 Mise : Multiplr: 1.00 IntFile Signal #1: EVENTS.E ' IntFile Signal #2: EVENTS.E Quant Time: Dec 10 13:04 2001 Quant Results File: 121001P.RES

Quant Method : C:\HPCHEM\1\METHODS\508\121001P.M (Chemstation Integrator) Title : 508 Chlorinated Pesticides Last Update : Thu Dec 06 15:08:51 2001 • Response via : Initial Calibration DataAcq Meth : PESTPCB.M

Volume Inj . Signal #1 Phase Signal #2 Phase: Signal #1 Info Signal #2 Info :

Compound RT#1 RT#2 Resp#l Resp#2 ug/1 ug/1

System Monitoring Compounds .0) S 2,4 DDD Surrogat 21.62 21.91 3733488 246851 0.142m 0.139m Spiked Amount 0.200 Recovery 71.00% 69.50%

Target Compounds 1) Propachlor 14.32 13.77 561137 49293 0.185m O.lSOm^^/* 2) g-BHC 16.48 16.21 15049127 892986 0.228 0.23 6m/<^4 3) Heptachlor 17.09 17.16 3501117 202259 0.074 0.018 m/Cf' 4) Aldrin 17.88 18.12 6451138 414209 0.097 0.096mX0/' 5) Heptachlor Epoxi 19.67 19.69 8772924 662359 0.206 0.195m/f/' 6) 4,4-DDE 20.89 21.22 13523964 904719 0.320 0.322m<^rA 7) Dieldrin 21.35 21.49 3064092 155720 0.066 0.067m-fQZ. 8) Endrin 21.90 22.47 4282166 294930 0.162 ■ 0.175m -WA—. 9) Methoxychlor 24.91 26.14 1447769 233209 ‘ 0.238m 0.316m^(^p

(f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int. 2PESTC2.D PCB1232.M Wed Dec 12 14:55:17 2001 Page 1

NYC-WTC_d6009i290

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NYC-WTC_000091290Source: NYC Law Department, mirrored locally

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