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← Document results/DEP Box 68/508 X 11/8/01 A 12/5/01
Document / 4 pages

Chlorinated pesticides chromatogram review, Dec 2001

Machine-extracted title · confidence 95%

Technical record of instrument signal review and data processing for chlorinated pesticide analysis conducted in December 2001.

NYC-WTC_000090646–000090649

Folder label: “508 X 11/8/01 A 12/5/01

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Scanned page image, NYC-WTC_000090648
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Signal #1 : C:\HPCHEM\1\DATA\5O81O4\O112O3\11O8REFT.D\ECD1A.CH Vial: 30 Signal #2 : C:\HPCHEM\l\DATA\508104\011203\1108REFT.D\ECD2B.CH Acq On : 4 Dec 2001 5:14 am Operator: Nefliu Sample : 11/08 ref tox Inst 104 Mise : Multiplr: I'.OO IntFile Signal #1: events.e IntFile Signal #2: events2.e Quant Time: Dec 20 10:01 2001 Quant Results File: 011205T.RES

Quant Method : C:\HPCHEM\1\METHODS\508104\011205T.M (Chemstation Integratoi Title : 508 CHLORINATED PESTICIDES TOXAPHENE7/28/99 Last Update : Fri Nov 09 16:13:01 2001 Response via : Initial Calibration DataAcq Meth : 508F2.M

Volume Inj. Signal #1 Phase Signal #2 Phase: Signal #1 Info Signal #2 Info :

Compound RT#1 RT#2 Resp#l Resp#2 ug/1 ug/1

System Monitoring Compounds 6) S 2,4-DDD SURROGAT 36.08 33.61 1339914 1232312 0.194m 0.172m Spiked Amount 0.200 Recovery 97.00% 86.00%

Target Compounds 1) TOXAPHENE PEAK 1 34.36 34.83 196460 195963 3.909m 4.196m 2) TOXAPHENE PEAK 2 38.07 36.32 916026 479619 4.486m 3.886m 3) TOXAPHENE PEAK 3 39.57 38.24 620279 229381 4.006m 2.653m# 4) TOXAPHENE PEAK 4 44.06 39.30 525977 208636 2.831m 1.918m# 5) TOXAPHENE PEAK 5 44.54 40.31 293344 205706 1.216m 2.206m#

(f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int. 1108REFT.D 011205T.M Thu Dec 20 10:01:17 2001 Page 1

NYC-WTC_000090648

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NYC-WTC_000090648Source: NYC Law Department, mirrored locally

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