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← Document results/DEP Box 68/508 X 11/8/01 A 12/5/01
Document / 7 pages

Chlorinated pesticides method validation data, Dec 2001

Machine-extracted title · confidence 95%

Laboratory report showing recovery percentages and relative standard deviations for chlorinated pesticide analysis methods.

NYC-WTC_000090635–000090641

Folder label: “508 X 11/8/01 A 12/5/01

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Scanned page image, NYC-WTC_000090636
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Signal #1 : C:\HPCHEM\1\DATA\508104\011203\TOXC1.D\ECD1A.CH Vial: 10 Signal #2 : C:\HPCHEM\1\DATA\508104\011203\TOXC1.D\ECD2B.CH Acq On : 3 Dec 2001 7:35 pm Operator: Nefliu Sample : tox id Inst 104 Mise : Multiplr: 1.00 IntFile Signal #1: events.e IntFile Signal #2: events2.e Quant Time: Dec 20 10:08 2001 Quant Results File: 011205T.RES

Quant Method : C:\HPCHEM\1\METHODS\508104\011205T.M (Chemstation Integrator Title : 508 CHLORINATED PESTICIDES TOXAPHENE7/28/99 Last Update : Fri Nov 09 16:13:01 2001 Response via : Initial Calibration DataAcq Meth : 508F2.M

Volume Inj. Signal #1 Phase Signal #2 Phase: Signal #1 Info Signal #2 Info :

Compound RT#1 RT#2 Resp#l Resp#2 ug/1 ug/1

System Monitoring Compounds 6) S 2,4-DDD SURROGAT 0.00 0.00 0 0 N.D. d N.D. d Spiked Amount 0.200 Recovery 0.00% 0.00%

Target Compounds 1) TOXAPHENE PEAK 1 34.34 34.84 33302 30567 0.663m 0.655m 2) TOXAPHENE PEAK 2 38.16 36.34 124697 81882 0.611m 0.663m 3) TOXAPHENE PEAK 3 39.55 38.25 92712 58054 0.599m 0.671m 4) TOXAPHENE PEAK 4 44.03 39.31 103534 61050 0.557m 0.561 5) TOXAPHENE PEAK 5 44.52 40.32 114650 52489 0.475m 0.563m

nr/- J

(f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int. TOXCl.D 011205T.M Thu Dec 20 10:10:11 2001 Page 1

NYC-WTC_000090636

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NYC-WTC_000090636Source: NYC Law Department, mirrored locally

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