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Document / 9 pages

Pesticide calibration verification results, sample AD26833, Dec 2001

Machine-extracted title · confidence 90%

Calibration data showing recovery percentages for various pesticide standards in sample AD26833.

NYC-WTC_000090612–000090620

Folder label: “508 X 11/8/01 A 12/5/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Signal #1 : C:\HPCHEM\l\DATA\508104\011203\PESTC2.D\ECDlA.CH Vial: 20 Signal #2 : C:\HPCHEM\l\DATA\508104\011203\PESTC2.D\ECD2B.CH Acq On : 4 Dec 2001 12:25 am Operator: Nefliu Sample : pest ic2 Inst : 104 Mise : Multiplr: 1.00 IntFile Signal #1: events.e IntFile Signal #2: events2.e Quant Time: Dec 18 15:34 2001 Quant Results File: 011205P.RES

Quant Method : C:\HPCHEM\1\METHODS\508104\011205P.M (Chemstation Integrator Title : 508 CHLORINATED PESTICIDES 9/6/00 Last Update : Sun Oct 21 15:26:52 2001 Response via : Initial Calibration DataAcq Meth : 508F2.M

Volume Inj. Signal #1 Phase Signal #2 Phase: Signal #1 Info Signal #2 Info :

Compound RT#1 RT#2 Resp#l Resp#2 ug/L ug/L

System Monitoring Compounds LO) S 2,4-DDD SURROGAT 36.07 33.62 1157705 1158723 0.199 0.195m Spiked Amount 0.200 Recovery 99.50% 97.50%

Target Compounds 1) PROPACHLOR 15.78 15.22 208711 211587 0.210 0.209 2) g-BHC 21.74 20.11 3086460 3775718 0.301 loS/x 0.286 3) HEPTACHLOR 24.33 21.49 729241 973302 0.099 tOV. 0.093 4) ALDRIN 27.04 23.52 1520153 1580662 0.129 0.120 5) HEPTACHLOR EPOXI 31.17 28.81 2587450 2807515 0.258 0.241 6) 4,4'-DDE 34.73 31.98 4290491 4677763 0.438m Ho/- 0.411 7) DIELDRIN 34.96 32.64 817690 925810 0.085m 0.080 8) ENDRIN 36.90 33.69 1220642 1903843 0.221 0.218m 9) METHOXYCHLOR 47.22 40.58 1049452 1209563 0.419 0.371

(f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int. PESTC2.D 011205P.M Tue Dec 18 15:35:08 2001 'Page 1

NYC-WTC_000090613

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NYC-WTC_000090613Source: NYC Law Department, mirrored locally

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