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GC/MS analysis results for sample AD23835, Nov 1 2001

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Laboratory report documenting GC/MS analysis of sample AD23835 conducted on November 1, 2001, identifying unknown compounds.

NYC-WTC_000089501–000089516

Folder label: “GC/MS Scan 10/1/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\OCT3001\23835.D Vial: 20 Acq On : 31 Oct 2001 9:02 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Oct 31 12:29 2001 Quant Results File: NP101901.RES Quant Method : C: \HPCHEM\1\METHODS\NP1019()1 .M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue Oct 23 10:12:13 2001 Response via : Initial Calibration DataAcq Meth : NP101901

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.72 152 570860 20.00 ug/1 -0.04 19) Naphthalene-d8 15.32 136 . 2280571 20.00 ug/l -0.04 31) Acenaphthene-dlO 20.59 164 1099207 20.00 ug/1 -0.04 49) Phenanthrene-dlO 25.02 188 1580741 20.00 ug/1 -0.04 59) Chrysene-dl2 33.06 240 978337 20.00 ug/1 -0.04 68) Perylene-dl2 37.15 264 684192 20.00 ug/1 -0.04 System Monitoring Compounds 4) 2-Fluorophenol 0.00 112 0 0.00 ug/1 Spiked Amount 75.000 . Recovery = 0.00% 5) Phenol-d5 0.00 99 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 6) 2-Chlorophenol-d4 11.72 132 336 0.01 ug/1 0.45 Spiked Amount 75.000 Recovery = 0.01% 7) 1,2-Dichlorobenzene-d4 12.23 152 6073 0.15 ug/1 -0.04 Spiked Amount 50.000 Recovery = 0.30% 20) Nitrobenzene-d5 0.00 82 0 0.00 ug/1 Spiked Amount 50.000 Recovery = 0.00% 32) 2-Fluorobiphenyl 18.61 172 231 0.00 ug/1 -0.04 Spiked Amount 50.000 Recovery = 0.00% 33) 2,4,6-Tribromophenol 0.00 33 0 . 0 0.00 ug/1 Spiked Amount 75.000 Recovery 0.00% 62) Terphenyl-dl4 0.00 244 0 0.00 ug/1 •y. Spiked Amount 50.000 Recovery = 0.00% Target Compounds Qvalue 2) Pyridine 0.00 79 0 N.D. 3) N-nitroso-dimethyl amine 0.00 74 - 0. N.D. 8) Phenol 0.00 94 0 N.D. 9) bis(2-Chloroethyl)ether 0.00 93 0 N.D. - 10) 2-Chlorophenol — - - — — -0.00- 128 — .__0—— N.D. - 11) 1,3-Dichlorobenzene 0.00 146 0 N.D. 12) 1,4-Dichlorobenzene 0.00 146' 0 N.D. T3)“1,2-Dichlorobenz ene- — - - o-.-oo 1-46-t— -^0— N.-D—* " 14)“2-MetHylpK^ol 'oTov "'m' 0 ■n.d. 15) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 16) 3&4-Methylphenol _ 0.00 108 0 N..D. i7) ,N-Nitroso-"di^n~prOpylamine 0.00 70 -0 ■■ NTD” 18) Hexachloroethane . 0.00 117 0 N.D. 21) Nitrobenzene 0.00 77 0 N.D. 22) Isophorone 0.00 82 0 N.D. (#) = qualifier out of range (m) = manual integration 23835.D NP101901.M Wed Oct 31 12:30:22 2001 Page 1 .

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