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GC/MS analysis results for sample AD23838, Nov 2 2001

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Laboratory report documenting GC/MS analysis of sample AD23838 conducted on November 2, 2001, identifying unknown compounds.

NYC-WTC_000089346–000089365

Folder label: “GC/MS Scan 10/1/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) I

Data File : C;\HPCHEM\1\DATA\OCT3001\23838.D Vial: 12 Acq On : 31 Oct 2001 1:15 am Operator: 209 GALOS Sample : gc/ms unknown Inst ; GC/MS 209 Mise : Multiplr; 1.00 MS Integration Params*. RTEINT.P Quant Time; Nov 2 10:06 2001 Quant Results File; NP101901.RES : Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue Oct 23 10:12:13 2001 Response via : Initial Calibration DataAcq Meth : NP101901

Compound R.T. Qlon Response Cone Unit Qvalue ’ 23) 2-Nitrophenol O.oo 139 0 N.D. 24) 2,4-Dimethylphenol 0.00 107 0 N.D. 25) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 26) 2,4-Dichlorophenol 0.00 162 0 N.D. 27) 1,2,4-Trichlorobenzene 0.00- 180 0 N.D. 28) Naphthalene 15.39 128 517 N.D. 29) Hexachlorobutadiene 0.00 225 0 N.D. 30) 4-Chloro-3-methylphenol 0.00 107 0 N.D. 34) Hexachlorocyclopentadiene 0.00 237 0 N.D. 35) 2,4,6-Trichlorophenol 0.00 196 0 N.D. 36) 2,4,5-Trichlorophenol 0.00 196 0 N.D. 37) 2-Chloronaphthalene 0 .'00 162 0 N.D. 38) Dimethylphthalate 0.00 163 0 N.D. 39) 2,6-Dinitrotoluene . 0.00 165 0 N.D. d 40) Acenaphthylene 0.00 152 0 N.D. 41) Acenaphthene 0.00 153 0 N.D. 42) 2,4-Dinitrophenol O.'OO 184 0 N.D. 43) 4-Nitrophenol 21.07 65 178 N.D. 44) 2,4-Dinitrotoluene 21.07 165 288 N.D. 45) Diethylphthalate 22.11 149 457 N.D. ■ 46) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 47) Fluorene 0.00 166 0 N.D. 48) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 50) 4,6-Dinitro-2-methylphenol 0.00 198 0- N.D. __ __51)_N-Nitrosodiphenylamine-— - __0.00^168v —-- 0^ -- N.-D-.-- 52) 4-Bromophenyl-phenylether 0.00 248 0 N.D. .i 53) Hexachlorobenzene 0.00 284 0 N.D. 54) Pentachlorophenol 0.00 266 0 N.D. 5 5) Phenanthrene 25.09 178 408 N.D. 56) Anthracene 25.09 178 408 N.D. ■_ 57) Di_-n7butylphthalate_ ____ ._27.03_T49__ -6226._ -N.D 5 8) Fluoranthene 28.70 202 180 N.D. 60) 3,3'-Dichlorobenzidine 0.00 252 0 N.D. _61)_Benzidine—— -___ __ —0.00—184—— — 0.— - --N-.Drr^ ■ —63)—Pyrene - - 0700-"=2 02=^ -0- - -NTD’-- 64) Butylbenzylphthalate 0.00 149 0 N.D. 65) Benzo(a)anthracene 0.00 228 0 N.D. d 66)—Bis-(2-ethy-l-hexyl.-)-phfeha-late .. O-.'OO —1-49' --- 0—- -- NvD—d- 67) Chrysene 0.00 228 0 N.D. d 69) Di-n-Octylphthalate 35.07 149 736 ' N.D. 70) Benzo(b)fluoranthene 36.09 252 1062 N.D. (#) = qualifier out of range (m) = manual integration 23838.D NP103001.M Fri Nov 02 10:07:03 2001 Page 2

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