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GC/MS analysis results for sample AD23837, Nov 1 2001

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Laboratory report documenting GC/MS analysis of sample AD23837 conducted on November 1, 2001, identifying unknown compounds.

NYC-WTC_000089333–000089345

Folder label: “GC/MS Scan 10/1/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\OCT3001\23837.D Vial: 11 Acq On : 31 Oct 2001 12:17 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 ' Mise : Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Oct 31 12:07 2001 Quant Results File: NP101901.RES Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration^ table Last Update : Tue Oct 23 10:12:13 2001 Response via : Initial Calibration DataAcq Meth : NP101901

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.71 152 1002890 20.00 ug/1 -0.04 . 19) Naphthalene-d8 15.32 136 3975940m 20.00 ug/1 - 0.04 31) Acenaphthene-dlO 20.60 164 1937289 20.00 ug/1 - 0.04 49) Phenanthrene-dlO 25.02 188 2786526m 20.00 'ug/1 -0.04 59) Chrysene-dl2 33.07 240 1744861m 20.00 ug/1 -0.04/. 68) Perylene-dl2 37.16 264 1258188 20.00 ug/1 -0.04 . System Monitoring Compounds 4) 2-Fluorophenol 0.00 112 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 5) Phenol-d5 0.00 99 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 6) 2-Chlorophenol-d4 0.00 132 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 7) 1,2-Dichlorobenzene-d4 12.23 152 11126 0.16 ug/1 -0.04 Spiked Amount 50.000 Recovery = 0.32% 20) Nitrobenzene-d5 0.00 82 0 0.00 ug/1 Spiked Amount 50.000 Recovery = 0.00% 32) 2-Fluorobiphenyl 18.74 172 4482 0.02 ug/1 0.09 .../ Spiked Amount 50.000 Recovery = 0.04% 33) 2,4,6-Tribromophenol 0.00 330 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 62) Terphenyl-dl4 0.00 244 . 0 0.00 ug/1 Spiked Amount 50.000 Recovery = 0.00% Target Compounds Qvalue' 2) Pyridine 0.00 79 0 N.D. 3) N-nitroso-dimethyl amine 0.00 74 . 0 N.D. 8) Phenol 0.00 94 . 0 N.D. 9) bis(2-Chloroethyl)ether 0.00 93 0 N.D. __10)_2-Chiprophenol 0.00 128_2_ _0,_„ __N.D__ 11) 1,3-bichlorobenzene 0.00 146 . 0 N.D. 12) 1,4-Dichlorobenzene 0.00 146 • 0 N.D. 13) 1,2-.Dichlorobenzene - 0.00 146 -- —0-^ —N. D . —14 )- -2-Methylphenol—" OvO 0-^108 — N:Dt— 15) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 16) 3&4-Methylphenol 0.00 108 0 N.D. 17)- N-Nitroso-di-n-propylami-he^^—0.00 • 70 ^O-- —NvDz-- 18) Hexachloroethane 0.00 117 0 N.D. 21) Nitrobenzene 0.00 77 0 . N.D. 22) Isophorone 0.00 82 0.. N.D. (#) = qualifier out of range (m) = manual integration 23837.D NP101901.M Wed Oct 31 12:08:00 2001 Page 1

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