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← Document results/DEP Box 67/GC/MS Scan 9/28/01
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GC/MS analysis report, sample AD23722, Oct 2001

Machine-extracted title · confidence 100%

Laboratory record for sample AD23722 showing detection of unknown compounds on October 17, 2001.

NYC-WTC_000089247–000089258

Folder label: “GC/MS Scan 9/28/01

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Scanned page image, NYC-WTC_000089249
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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\OCT1501\23722.D Vial: 18 Acq On : 16 Oct 2001 4:48 am Operator: 209 GALOS Sample : gc/ms unknown Inst ; GC/MS 209 Mise : Multiplr; 1.00 MS Integration Params: RTEINT.P Quant Time: Oct 16 14:41 2001 Quant Results File: NP091101.RES Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Last Update : Fri Oct 12 09:04:47 2001 Response via : Initial Calibration DataAcq Meth : NP091101

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.76 152 ■343703 20.00 ug/1 -0.15 19) Naphthalene-d8 15.38 136 134257'9 20.00 ug/1 -0.15 31) Acenaphthene-dlO 20.65 164 63'5246 20.00 ug/1 -0.16 49) Phenanthrene-dlO 25.08 188 896265 20.00 ug/1 -0.16 59) Chrysene-dl2 33.12 240 606848 20.00 ug/1 -0.16 68) Perylene-dl2 37.23 264 418626 20.00 ug/1 -0.19 System Monitoring Compounds 4) 2-Fluorophenol 0.00 112 0; 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 5) Phenol-d5 0.00 99 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 6) 2-Chlorophenol-d4 0.00 132 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 7) 1,2-Dichlorobenzene-d4 12.28 152 3459 0.21 ug/1 -0.15 Spiked Amount 50.000 Recovery = 0.42% 20) Nitrobenzene-d5 0.00 82 0 0.00 ug/1 Spiked Amount 50.000 Recovery = 0.00% 32) 2-Fluorobiphenyl 18.80 172 1269' 0.03 ug/1 -0.01 Spiked Amount 50.000 Recovery = 0.06% 33) 2,4,6-Tribromophenol 0.00 330 0.00 ug/1 Spiked Amount 75.000 Recovery 0.00% 62) Terphenyl-dl4 0.00 244 • ■ ■ b.OO ug/1 0. ■

Spiked Amount 50.000 Recovery = 0.00% Target Compounds Qvalue 2) Pyridine 0.00 79 -0-- ' N.D. 3) N-nitroso-dimethyl amine 0.00 74 ■ 0 . N.D. 8) Phenol 0.00 94 0 N.D. 9) bis(2-Chloroethyl)ether 0.00 93 . 0’ N.D. 10). _2-Chlorophenol_ 0.00 128 -^-:0^ — N.D. - 11) 1,3-Dichlorobenzene 0.00 146 0 N.D. 12) 1,4-Dichlorobenzene 0.00 146 •0 . N.D. .^^-13 j—1 ,-2 - D i chlor ob enz ene------ rz.- .-^OwO.O.- -146 - --r-0--- -r-^N-rD— ^^=T4-)" 2 - M e t hy IpKeiioi -^=0t0’0=^1’0’8’^- -- NTD— 15) 2,2'-oxybis(1-Chloropropan 0.00 45 . ■ .-.0 ■■ N.D. 16) 3&4-Methylphenol 0.00 108 0 . N.D. -1-7-) - -N- Ni hr o s o - di- n - p ropy l-amine- OvOO -70 --- NtD~ 18) Hexachloroethane o'. 00 117 . 6 ■ N.D. 21) Nitrobenzene 0.00 77 ■ 0:. • N.D. 22) Isophorone 0.00 82 O' N.D. (#) = qualifier out of range (m) = manual integration 23722.D NP091101.M Tue Oct 16 14:43:03 2001 Page 1

NYC-WTC_000089249

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NYC-WTC_000089249Source: NYC Law Department, mirrored locally

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