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GC/MS analysis report, sample AD23719, Oct 2001

Machine-extracted title · confidence 100%

Laboratory record for sample AD23719 showing detection of unknown compounds on October 17, 2001.

NYC-WTC_000089203–000089217

Folder label: “GC/MS Scan 9/28/01

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Scanned page image, NYC-WTC_000089205
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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\OCT1501\23719.D Vial: 15 Acq On : 16 Oct 2001 1:53 am Operator; 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Oct 16 14:39 2001 Quant Results File; NP091101.RES Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Last Update : Fri Oct 12 09:04:47 2001 Response via : Initial Calibration DataAcq Meth : NP091101

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.77 152 387422 20.00 ug/1 -0.14 - . 19) Naphthalene-d8 15.37 136 1496769 20.00 ug/1 -0.15/'. 31) Acenaphthene-dlO 20.65 164 703171 20.00 ug/1 -0.16 49) Phenanthrene-dlO 25.09 188 1032528 20.00 ug/1 -0.15 59) Chrysene-dl2 33.12 240 727720 20.00 ug/1 -0.16 \ 68) Perylene-dl2 37.23 264 529391 20.00 ug/1 -0.19 System Monitoring Compounds 4) 2-Fluorophenol 0.00 112 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 5) Phenol-d5 0.00 99 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 6) 2-Chlorophenol-d4 11.77 132 216 0.01 ug/1 0.35 Spiked Amount 75.000 Recovery = 0.01% 7) 1,2-Dichlorobenzene-d4 12.28 152 3835 0.20 ug/1 -0.15 Spiked Amount 50.000 Recovery = 0.40% 20) Nitrobenzene-d5 0.00 82 0 0.00 ug/1 Spiked Amount 50.000 Recovery = 0.00% 32) 2-Fluorobiphenyl 18.81 172 1253 0.03 ug/1 0.00 Spiked Amount 50.000 Recovery = 0.06% 33) 2,4,6-Tribromophenol 0.00 330 0 0.00 ug/1 Spiked Amount 75.000 Recovery 0.00% 62) Terphenyl-dl4 0.00 244 0 0.00 ug/1 Spiked Amount 50.000 Recovery = 0.00% Target Compounds Qvalue 2) Pyridine 0.00 79 0 N.D. 3) N-nitroso-dimethyl amine 0.00 74 0 N.D. 8) Phenol 0.00 94 0 N.D. 9) bis(2-Chloroethyl)ether 0.00 93 0 . N.D. _ .10)—2-Chlorophenol -- - —.— — -0.00- -128 - • 0 - N-.D. 11) 1,3-Dichlorobenzene 0.00 146 0 N.D. 12). 1,4-Dichlorobenzene 0.00 146 0 N.D. —1-3-) —1-/2 -Di-chlorobenzene -- -.' - - -- OtOO—1-4-6—- —‘0' •NxD-- —T'4')“2 -Methylphenol ~ ■- 070'0—1’0'8— 'N7D~~ 15) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 16) 3 &4-Methylphenol 0.0 0_ 108 0 N.D. ---17)—N-Nitroso=-di—n-=propyl"amine ’ '"’OTO O" -70 —-0“ ‘N7DT— 18) Hexachloroethane 0.00 117 0 N.D. . 21) Nitrobenzene 0.00 77 0 N.D. 22) Isophorone 0.00 82 0 N.D. (#) = qualifier out of range (m) = manual integration 23719.D NP091101.M Tue Oct 16 14:45:24 2001 Page 1 .

NYC-WTC_000089205

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NYC-WTC_000089205Source: NYC Law Department, mirrored locally

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