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GC/MS analysis report, sample AD23717, Oct 2001

Machine-extracted title · confidence 100%

Laboratory record for sample AD23717 showing detection of unknown compounds on October 17, 2001.

NYC-WTC_000089171–000089184

Folder label: “GC/MS Scan 9/28/01

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Scanned page image, NYC-WTC_000089173
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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\OCT1501\23717.D Vial: 13 Acq On : 15 Oct 2001 11:56 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Oct 16 14:39 2001 Quant Results File: NP091101.RES Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Last Update : Fri Oct 12 09:04:47 2001 Response via : Initial Calibration DataAcq Meth : NP091101

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.76 152 355341 20.00 ug/1 -0.14 19) Naphthalene-d8 15.37 136 1392995 20.00 ug/1 -0.15 31) Acenaphthene-dlO 20.66 164 658190 20.00 ug/1 -0.15 49) Phenanthrene-dlO 25.09 188 945183 20.00 ug/1 -0.15 59) Chrysene-dl2 33.12 240 674856 20.00 ug/1 -0.16 68) Perylene-dl2 37.23 264 490049 20.00 ug/1 -0.19 System Monitoring Compounds 4) 2-Fluorophenol 0.00 112 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 5) Phenol-d5 0.00 99 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 6) 2-Chlorophenol-d4 0.00 132 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 7) 1,2-Dichlorobenzene-d4 12.28 152 3606 0.21 ug/1 -0.15 Spiked Amount 50.000 Recovery = 0.42% 20) Nitrobenzene-d5 0.00 82 0 . 0.00 ug/1 Spiked Amount 50.000 Recovery = 0.00% 32) 2-Fluorobiphenyl 18.81 172 1272 0.03 ug/1 0.00 Spiked Amount 50.000 Recovery = 0.06% 33) 2,4,6-Tribromophenol 0.00 330 0 0.00 ug/1 Spiked Amount’ 75.000 Recovery = 0.00% 62) Terphenyl-dl4 0.00 244 0 6.00 ug/1 Spiked Amount 50.000 Recovery = 0.00% Target Compounds Qvalue 2) Pyridine 0.00 79 0 N.D. 3) N-nitroso-dimethyl amine 0.00 74 0 N.D. 8) Phenol 0.00 94 0 N.D. 9) bis(2-Chloroethyl)ether 0.00 93 0 N.D. _10) 2-Chlorophenol. , -0.00__128 .0—. --- N-.D.- 11) 1,3-Dichlorobenzene 0.00 146 0 N.D. 12) 1,4-Dichlorobenzene 0.00 146 0 -N.D. —.13)—:l-,-2-DiGhlorobenzene —r - —— —0%-00—rl46 —<f7NvD-;- —T4-)=2'- M e thy ipherrdi=======^^ — ==0T0'0—IW ”0"— —NTDT I 15) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 16) 3&4-Methylphenol 0.00 108 0 N.D. -1-7-)—N-Ni-troso -di-^-pr opylamine- - — OvO 0- ^7-0- “O'— —-N-D-.- 18) Hexachloroethane’ 0.00 117 0 N.D. 21) Nitrobenzene 0.00 77 0 N.D. 22) Isophorone 0.00 82 0 N.D. {#) = qualifier out of range (m) = manual integration 23717.D NP091101.M Tue Oct 16 14:47:50 2001 Page 1

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NYC-WTC_000089173Source: NYC Law Department, mirrored locally

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