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GC/MS analysis results for sample AD23650, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD23650 conducted on October 19, 2001.

NYC-WTC_000089000–000089024

Folder label: “GC/MS Scan 9/27/01

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NYC 9/11 Public Portal Document

LSC Area-Percent—Report-- Data File : C:\HPCHEM\1\DATA\OCT1601\23650.D Vial: 15 Acq On : 17 Oct 2001 3:56 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 6.394 143 147 152 rBV 24165 46710 1.60% 0.282% 2 6.495 154 158 168 rW 39693 98770 3.38% 0.595% 3 6.632 169 173 179 rW 18789 39011 1.34% 0.235% 4 6.743 181 185 192 rW 26688 55877 1.91% 0.337% 5 11.626 712 717 726 rBV 24885 56784 1.94% 0.342%

6 11.764 726 732 749 rBV 872764 2079357 71.19% 12.532% 7 15.372 1118 1125 1142 rBV 1204853 2839443 97.22% 17.113% 8 20.660 1693 1701 1715 rBV 1274127 2920653 100.00% 17.603% 9 25.085 2176 2183 2196 rBV 1267153 2722709 93.22% 16.410% 10 29.510 2660 2665 2672 rBV 76861 141555 4.85% 0.853%

11 29.629 2672 2678 2684 rW 26432 51946 1.78% 0.313% 12 30.703 2791 2795 2802 rBV2 41175 77706 2.66% 0.468% 13 31.649 2892 2898 2903 rBV 50601 102147 3.50% 0.616% 14 31.741 2903 2908 2918 rVB 80815 168577 5.77% l-.016% 15 32.732 3009 3016 3028 rBV 77197 163992 5.61% 0.988%

.. 16 .33.127__3 051_3 059-3 074_rBV—1045054 -2432747.—83 ..29%-- 14-.-66-2%- 17 33.687 3112 3120 3130 rBV 86366 188790 6.46% 1.138% 18 34.614 3216 3221 3231 rVB 62852 133813 4.58% 0.806% 19 35.504 3312 3318 3329 rBV 45381 106543 3.65% 0.642% 20 36.367 3405 3412 3418 rBV 22725 60399 2.07% 0.364%

21 37.230 3498 3506 3525 rBV2_. 713073 2104647 72.06% 12.685% _

Sum of.-corrected areas.:— 16592176-- 23650.D NP091101.M Thu Oct 18 10:39:57 2001

NYC-WTC_000089005

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NYC-WTC_000089005Source: NYC Law Department, mirrored locally

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