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GC/MS analysis results for sample AD23650, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD23650 conducted on October 19, 2001.

NYC-WTC_000089000–000089024

Folder label: “GC/MS Scan 9/27/01

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NYC 9/11 Public Portal Document

I Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\OCT1601\23650.D Vial: 15 Acq On : 17 Oct 2001 3:56 am Operator: 2 09 GTkLOS Sample : gc/ms unknown Inst ; GC/MS 209 Mise : Multiplr; 1.00 MS Integration Params: RTEINT.P Quant Time: Oct 18 11:35 2001 Quant Results File: NP091101.RES Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Last Update : Fri Oct 12 09:04:47 2001 Response via : Initial Calibration DataAcq Meth : NP091101

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.76 152 396984 20.00 ug/1 -0.14 19) Naphthalene-d8 15.37 136 1541587m 20.00 ug/1 -0.15 31) Acenaphthene-dlO 20.66 164 737341 20.00 ug/1 -0.15 49) Phenanthrene-dlO 25.08 188 1078455 20.00 ug/1 -0.15 59) Chrysene-dl2 33.13 240 791085 20.00 ug/1 -0.15 68) Perylene-dl2 37.24 264 577095 20.00 ug/1 -0.18

System Monitoring Compounds 4) 2-Fluorophenol 0.00 112 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 5) Phenol-d5 0.00 99 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 6) 2-Chlorophenol-d4 0.00 132 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 7) 1,2-Dichlorobenzene-d4 12.28 152 4166 0.22 ug/1 -0.15 Spiked Amount 50.000 Recovery = 0.44% 20) Nitrobenzene-d5 0.00 82 0 0.00 ug/1 Spiked Amount 50.000 Recovery = 0.00% 32) 2-Fluorobiphenyl 18.80 172 1456 0.03 ug/1 -0.01 Spiked Amount 50.000 Recovery = 0.06% 33) 2,4,6-Tribromophenol 0.00 330 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 62) Terphenyl-dl4 30.00 244 392- 0.01 ug/1 -0.15 -Spiked Amount--- 50.000- - -Recovery- - 0-^ 02% Target Compounds Qvalue 2) Pyridine 0.00 79 0 N.D. 3) N-nitroso-dimethyl amine 0.00 74 0 N.D. 8) Phenol 0.00 94 0 N.D. 9) bis(2-Chloroethyl)ether 0.00 93 0. N.D. 10) 2-Chlorophenol 0.00 128 0 N.D. 11) 1,3-Dichlorobenzene 0.00 146 0 N.D. _12i, 1,4-Dichlorobenzene _ _0-00—146— . - 0— N.D.- 13) 1,2-Dichlorobenzene “ O.-OO -146 -0-^^ N.D. 14) 2-Methylphenol 0.00 108 0 N.D. 15) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 16)—3&4-Methy-lphenol 0.00 -108- __o— N.D. 17) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 18) Hexachloroethane . 0.00 117 0 N.D. 21) Nitrobenzene 0.00 77 0 N.D. 22) Isophorone 0.00 82 0 N.D.

(#) = qualifier out of range (m) = manual integration 23650.D NP091101.M Thu Oct 18 11:35:52 2001 Page 1

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