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GC/MS analysis results for sample AD23607, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD23607 conducted on October 19, 2001.

NYC-WTC_000088986–000088999

Folder label: “GC/MS Scan 9/27/01

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NYC 9/11 Public Portal Document

Quant i tat ion-Report (QT Reviewed) Data File ; C:\HPCHEM\1\DATA\OCT1601\23607.D Vial: 14 Acq On : 17 Oct 2001. 2:57 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Oct 17 10:00 2001 Quant Results File: NP091101.RES Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Last Update : Fri Oct 12 09:04:47 2001 Response via : Initial Calibration DataAcq Meth : NP091101

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.76 152 388803 20.00 ug/1 -0.15 19) Naphthalene-d8 15.38 136 1532925 20.00 ug/1 -0.15 31) Acenaphthene-dlO 20.66 164 721278 20.00 ug/1 -0.16 49) Phenanthrene-dlO 25.08 188 1048552 20.00 ug/1 -0.16 59) Chrysene-dl2 33.12 240 738370 20.00 ug/1 -0.16 68) Perylene-dl2 37.24 264 547329 20.00 ug/1 -0.18 . System Monitoring Compounds 4) 2-Fluorophenol 0.00 112 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 5) Phenol-d5 0.00 99 0 0.00 ug/1 Spiked Amount • 75.000 Recovery = 0.00% 6) 2-Chlorophenol-d4 0.00 132 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 7) 1,2-Dichlorobenzene-d4 12.28 152 3930 0.21 ug/1 -0.15 Spiked Amount 50.000 Recovery = 0.42% 20) Nitrobenzene-d5 0.00 82 0 0.00 ug/1 Spiked Amount 50.000 Recovery = 0.00% 32) 2-Fluorobiphenyl 18.80 172 1486 0.03 ug/1 0.00 Spiked Amount 50.000 Recovery = 0.06% 33) 2,4,6-Tribromophenol 0.00 330 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 62) Terphenyl-dl4 0.00 244 0’ 0.00 ug/1 -Spiked-Amount--- 50.000 -Recovery-- = 0^ 00% Target Compounds Qvalue 2) Pyridine 0.00 79 0 N.D. 3) N-nitroso-dimethyl amine 0.00 74 0 N.D. 8) Phenol 0.00 94 .0 N.D. 9) bis(2-Chloroethyl)ether 0.00 .93- . 0 N.D. 10) 2-Chlorophenol 0.00 128 0 N.D. 11) 1,3-Dichlorobenzene 0.00 146 0 N.D. 12) 1-, 4.^Dichlorobenzene 0.00 146— — 0— -N.D-. 13) 1;'2-Dichlorobenzene =— 0.00 146-- - -0 " N’.D. 14) 2-Methylphenol 0.00 108 0 N.D. 15) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 16) 3 &4-Methylphenol -------- 0.00 108 -■ 0 “ NrDT 17) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 18) Hexachloroethane 0.00 117 0 N.D. 21) Nitrobenzene 0.00 77 0 N.D. 22) Isophorone 0.00 82 0 N.D. (#) = qualifier out of range (m) = manual integration 23607.D NP091101.M Wed Oct 17 10:00:51 2001 Page 1. .•

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