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GC/MS analysis results for sample AD23606, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD23606 conducted on October 19, 2001.

NYC-WTC_000088961–000088985

Folder label: “GC/MS Scan 9/27/01

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NYC 9/11 Public Portal Document

—Quantitation"Report (QT Reviewed)' “Dat'a~File : C: \HPCHEM\ 1 \DA'TA\OCT1 6 01 \ 2 3 6 0 6 . D Vial: 13 Acq On : 17 Oct 2001 1:59 am Operator: 209 GALOS Sample ; gc/ms unknown Inst : GC/MS 209. Mise Multiplr; 1,00 MS Integration Params:.RTEINT.P Quant Time: Oct 17 12:06 2001 Quant Results File: NP091101.RES Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Last Update : Fri Oct 12 09:04:47 2001 Response via : Initial Calibration DataAcq Meth : NP091101

Internal Standards R.T. Qlon Response Cone Units Dev(Min) Y 1) 1,4-Dichlorobenzene-d4 11.76 152 386881 20.00 ug/1 -0.15 . 19) Naphthalene-d8 15.38 136 1513089 20.00 ug/1 -0.15 31) Acenaphthene-dlO 20.66 164 708475 . 20.00 ug/1 -0.16 49) Phenanthrene-dlO 25.08 188 1040624 20.00 ug/1 -0.16 59) Chrysene-dl2 33.12 240 784517 20.00 ug/1 -0.16,. . 68) Perylene-dl2 37.24 264 577164 20.00 ug/1 -0.18' . System Monitoring Compounds 4) 2-Fluorophenol 0.00 112 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 5) Phenol-d5 0.00 99 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 6) 2-Chlorophenol-d4 0.00 132 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 7) 1,2-Dichlorobenzene-d4 12.28 152 4171 0.22 ug/1 -0.15 Spiked Amount 50.000 Recovery = 0.44% 20) Nitrobenzene-d5 0.00 82 0 0.00 ug/1 Spiked Amount 50.000 Recovery = 0.00% 32) 2-Fluorobiphenyl 18.80 172 1537 0.03 ug/1 0.00. Spiked Amount 50.000 Recovery = 0.06% 33) 2,4,6-Tribromophenol 0.00 330 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 62) Terphenyl-dl4 0.00 244 0 0.00 ug/1 Spiked Amount 50.000 Recovery = 0.00% -Target”Compounds* ~ Qvalue'. ■ 2) Pyridine 0.00 79 0 N.D. 3) N-nitroso-dimethyl amine 0.00 74 0 N.D. 8) Phenol 0.00 94 0 N.D. 9) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 10) 2-Chlorophenol 0.00 128 0 N.D. 11) 1-3-Dichlorobenzene 0.00 146 0 N7D. ■ 12) 1,4-Dichlorobenzene 0.00 146 0 N.D. 13) 1,2-Dichlorobenzene 0.00 146 0 *14)222-Methylphenol 7'7-7--. " 0.00L._T08 'o' __ N.D__ 15 ) 2 72*' - oxybis" (1’- Chloropropan 0.00 45 0 N.D. 16) 3&4-Methylphenol 0.00 108 0 ■ N.D. 17) N-Nitroso-di-n-propylamine 0.00 _ 70 0 ___N..D.._ 18) Hexachlordethane o.bo 117 0 N.D. 21) Nitrobenzene 0.00 77 0 N.D. 22) Isophorone 0.00 82 0 N.D. (#) = qualifier out of range (m) = manual integration 23606.D NP091101.M Thu Oct 18 09:51:34 2001 Page 1

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