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GC/MS analysis results for sample AD23499, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23499 conducted on October 19, 2001.

NYC-WTC_000088799–000088825

Folder label: “GC/MS Scan 9/27/01

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NYC 9/11 Public Portal Document

i'. Quantitation Report (-QT-Reviewed) Data File C; \HPCHEM\1\DATA\OCT1601\23499 .D Vial: 7 Acq On : 16 Oct 2001 8:06 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P. Quant Time: Oct 17 12:03 2001 Quant Results File: NP091101.RES Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Last Update : Fri Oct 12 09:04:47 2001 Response via : Initial Calibration DataAcq Meth : NP091101

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.76 152 ■ 387697 20.00 ug/1 -0.15 19) Naphthalene-d8 .15.38 136 1531238 20.00 ug/1 -0.15 31) Acenaphthene-dlO 20.66 164 721606 20.00 ug/1 -0.16 49) Phenanthrene-dlO 25.08 188 1046048 20.00 ug/1 -0.16 59) Chrysene-dl2 33.12 240 785791 20.00 ug/1 -0.16 68) Perylene-dl2 37.24 264 582566 20.00 ug/1 -0.18

System Monitoring Compounds 4) 2-Fluorophenol 0.00 112 0 ' 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 5) Phenol-d5 0.00 99 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 6) 2-Chlorophenol-d4 0.00 132 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 7) 1,2-Dichlorobenzene-d4 12.27 152 3837 0.20 ug/1 -0.16 Spiked Amount 50.000 Recovery = 0.40% 20) Nitrobenzene-d5 0.00 82 0 0.00 ug/1 Spiked Amount 50.000 Recovery = 0.00% 32) 2-Fluorobiphenyl 18.80 172 1459 0.03 ug/1 0.00 Spiked Amount 50.000 Recovery = 0.06% 33) 2,4,6-Tribromophenol 0.00 330 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 62) Terphenyl-dl4 0.00 244 0 0.00 ug/1 Spiked Amount .50..-0.0.0. Recovery- —=---- 0”0-0%- Target Compounds Qvalue■ 2) Pyridine 0.00 79 0 - N.D. 3) N-nitroso-dimethyl amine 0.00 74 .0 - ■ N.D. 8) Phenol 0.00 94 0 : N.D. 9) bis(2-Chloroethyl)ether 0.00 93 0- -N.D.- 10) 2-'Chl6rophenol 0.00 128 0 N.D. 11) 1,3-Dichlorobenzene 0.00 146 0 N.D. 12)_ 1,4-Dichlorobenzene -146 _____ 0- 00^ 0 ■- —N-.-Dv- .13.).—1.,.2 -Dichlorobenzene------ - 0.00—146— 0 •- - n:d\’ 14) 2-Methylphenol 0.00 108 0 N.D. 15) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. _ .16 )__3&4-Methylphenol.— 0.00—108- 0 ' NtDt 17) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 18) Hexachloroethane 0.00 117 0 N.D. 21) Nitrobenzene 0.00 77 0 N.D. 22) Isophorone 0.00 82 0 . N.D. (#) = qualifier out of range (m) = manual integration 23499.D NP091101.M Thu Oct 18 09:46:28 2001 Page 1

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