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GC/MS analysis results for sample AD23272, Oct 15 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of environmental sample AD23272 conducted on October 15, 2001.

NYC-WTC_000088456–000088484

Folder label: “GC/MS Scan 9/25/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report 'Data File : C:\HPCHEM\1\DATA\OCT1201\23272.D vial: 22 Acq On : 12 Oct 2001 10:39 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 6.378 143 146 154 rBV 19871 43721 1.65% 0.224% 2 6.488 154 158 161.rBV 30757 59034 2.23% 0.302% 3 6.617 169 172 180 rVB 18605 36556 1.3 8% 0.187% 4 6.736 181 185 192 rVB 24264 50535 1.91% 0.258% 5 11.629 713 718 727 rVB 19433 47228 1.78% 0.241%

6 11.767 727 733 751 rBV 737616 1881162 70.94% 9.618% 7 15.375 1120 1126 1143 rBV 1138203 2595874 97.90% 13.272% 8 20.653 1694 1701 1715 rBV 1202669 2651675 100.00% 13.557% 9 25.078 2177 2183 2196 rBV2 1131187 2433664 91.78% 12.442% 10 27.318 r^2421 2427 2433 rVB 15648 31375 1.18% 0.160%

11 29.512 2660 2666 2673 rBV 473794 965628 36.42% 4.937% 12 29.622 2673 2678 2686 rW 96486 189746 7.16% 0.970% 13 29.751 2687 2692 2701 rVB 60392 118588 4.47% 0.606% 14 30.697 2790 2795 2803 rBV 139766 289040 10.90% 1.478% 15 31.642 2892 2898 2904 rBV 384036 754481 28.45% 3.857%

16 31.734 2904 2908 2917 rW 273095 560608 21.14% 2.866% 17 31.862 2918 2922 2931 rVB 23442 55072 2.08% 0.282% 18 32.725 3010 3016 3030 rBV 269321 568623 21.44% 2 .'907% 19 33.120 3052 3059 3073 rBV2 934817 2141585 80.76% 10.949% 20 33.689 3113 3121 3134 rBV 304940 656380 24.75% 3.356%

21 34.607 3213 3221 3234 rBV 223385 506473 19.10% 2.589% 22 35.498 3312 3318 3328 rBV 183041 421490 15.90% 2.155% 23 36.361 3406 3412 3425 rBV 100736 272186 10.26% 1.392% 24 37.233'^3498 3507 3512 rBV 661961 1901706 71.72% 9.723% 25 37.288 3512 3513 3525 rVB2 69506 176307 6.65% 0.901%

26 38.362 3623 3630 3638 rBV2 22947 85989 3.24% 0.440% 27 39.611 3756 3766 3774 rBV3 14105 64842 2.45% 0.332%

Sum of corrected areas: 19559568

23272.D NP091101.M Mon Oct 15 09:41:42 2001

NYC-WTC_000088461

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NYC-WTC_000088461Source: NYC Law Department, mirrored locally

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