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GC/MS analysis results for sample AD23324, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23324 conducted on October 15, 2001.

NYC-WTC_000088316–000088345

Folder label: “GC/MS Scan 9/25/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : C:\HPCHEM\1\DATA\OCT1201\23324.D Vial: 17 Acq On : 12 Oct 2001 5:46 pm Operator; 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params; LSCINT.P Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title ; 209 625/TCLP calibration table 7/16/01 Smoothing : OFF Filtering; 5 Sampling .- 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location; TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal ; TIC

peak R.T. first max last PK peak peak peak % Of # min scan scan scan TY height area % max. total 1 6.388 143 147 154 rBV 23048 43520 1.54% 0.200% 2 6.489 154 158 168 rVV2 37634 95898 3.40% 0.440% 3 6.627 169 173 178 rW 23476 46796 1.66% 0.215% 4 6.737 181 185 195 rVB2 33245 69602 2.47% 0.320% 5 11.621 712 717 727 rBV 23249 51977 1.84% 0.239% 6 11.759 727 732 753 rW 847614 2000885 70.93% 9.189% 7 15.376 1119 1126 1143 rBV 1143040 2753745 97.63% 12.647% 8 20.654 1693 1701 1719 rBV 1255942 2820732 100.00% 12.955% 9 25.079 2176 2183 2196 rBV2 1208195 2672171 94.73% 12.273% 10 27.319 2423 2427 2434 rVB 24462 48815 1.73% 0.224% 11 29.504 2660 2665 2673 rBV 493790 1008204 35.74% 4.630% 12 29.623 2673 2678 2683 rW 128753 252287 8.94% 1.159% 13 29.752 2686 2692 2703 rVB 77639 150194 5.32% 0.690% 14 30.698 2790 2795 2805 rVB 185444 381986 13.54% 1.754% 15 31.643 2892 2898 2904 rBV 389581 779184 27.62% 3.579% 16 31.735 2904 2908 2917 rW 355931 732109 25.95% 3.362% 17 31.863 2918 2922 2932 rVB 31138 . 70863 2.51% 0.325% 18 32.726 3011 3016 3024 rBV 339447 744356 26.39% 3.419% 19 33.121 3052 3059 3072 rBV2 1020852 2268008 80.40% 10.416% 20 33.690 3113 3121 3133 rBV 405243 847478 30.04% 3.892%

21 34.608 3213 3221 3236 rBV 296109 649044 23.01% 2.981% 22 35.499 3313 3318 3329 rBV 246059 552221 19.58% 2.536% 23 36.362 3405 3412 3426 rBV 138154 357203 12.66% 1.641% 24 37.234 3498 3507 3511 rBV2 680228 1876987 66.54% 8.620% 25 37.298 3511 3514 3526 rVB 93648 269858 9.57% 1.239% 26 38.363 3622 3630 3644 rBV 35077 142645 5.06% 0.655% 27 39.612 3758 3766 3774 rBV3 19570 86865 3.08% 0.399%

Sum of corrected areas: 21773633 23324.D NP091101.M Mon Oct 15 10:33:14 2001

NYC-WTC_000088321

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NYC-WTC_000088321Source: NYC Law Department, mirrored locally

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