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GC/MS analysis results for sample AD23322, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23322 conducted on October 15, 2001.

NYC-WTC_000088263–000088289

Folder label: “GC/MS Scan 9/25/01

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Scanned page image, NYC-WTC_000088268
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NYC 9/11 Public Portal Document

LSC Area Percent Report 'Data File : C:\HPCHEM\1\DATA\OCT1201\23322.D Vial; 15 Acq On : 12 Oct 2001 3:48 pm Operator: 2 09 GTkLOS Sample : gc/ms unknown Inst ; GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title ; 209 625/TCLP calibration table 7/16/01 Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs; 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location; TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal ; TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 6.378 142 146 152 rBV 23864 46979 1.68% 0.261% 2 6.479 153 157 169 rVV2 35948 96831 3.47% 0.538% 3 6.617 169 172 18 0 rW 21341 43429 1.56% 0.241% 4 6.727 180 184 194 rVB 26132 60922 2.18% 0.339% 5 11.630 713 718 727 rBV 22177 50469 1.81% 0.280% 6 11.767 727 733 748 rBV 793217 1962259 70.38% 10.905% 7 15.375 1119 1126 1142 rBV 1196541 2706318 97.06% 15.040% 8 20.654 1694 1701 1713 rBV 1272821 2788197 100.00% 15.495% 9 25.079 2176 2183 2195 rBV2 1172483 2582342 92.62% 14.351% 10 29.504 2659 2665 2673 rBV 381893 768467 27.56% 4.271%

11 29.623 2673 2678 2683 rW 73377 146450 5.25% 0.814% 12 29.751 2687 2692 2700 rVB2 45944 92453 3.32% 0.514% 13 30.697 2787 2795 2804 rBV 110730 224871 8.07% 1.250% 14 31.643 2893 2898 2904 rBV 288048 570308 20.45% 3.169% 15 31.734 2904 2908 2918 rW 208233 428389 15.36% 2.381% 16 31.863 2918 2922 2929 rVB2 17869 39827 1.43% 0.221% 17 32.726 3011 3016 3023 rBV 197392 405997 14.56% 2.256% 18 33.121 3052 3059 3070 rBV2 916596 2085862 74.81% 11.592% 19 33.690 3108 3121 3131 rBV 203837 462773 16.60% 2.572% 20 34.608 3213 3221 3230 rBV 144366 ■ 309926 11.12% 1.722%

21 35.498 3312 3318 3328 rBV 107391 244993 8.79% 1.361% 22 36.361 3407 3412 3420 rBV 54111 136305 4.89% 0.757% 23 37.224 3498 3506 3512 rBV2 610775 1699878 60.97% 9.447% 24 38.363 3625 3630 3639 rBV4 11745 40291 1.45% 0.224%

Sum of corrected areas: 17994536

23322.D NP091101.M Mon Oct 15 10:25:41 2001

NYC-WTC_000088268

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NYC-WTC_000088268Source: NYC Law Department, mirrored locally

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