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GC/MS analysis results for sample AD23262, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD23262 conducted on October 12, 2001.

NYC-WTC_000088115–000088179

Folder label: “GC/MS Scan 9/24/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) •Data File : C:\HPCHEM\1\DATA\OCT1101\23263.D Vial: 3 'Acq On : p<tJcE~^01 11:22 am Operator: 209 GALOS Sample :/reinject) Inst : GC/MS 209 Mise Multiplr: 1.00 MS IntegraK^n Params: RTEINT.P Quant Time: cur'll 12:11 2 001 Quant Results File: NP091101.RES Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Last Update : Thu Sep 13 12:47:04 2001 Response via : Initial Calibration DataAcq Meth : NP091101

Internal Standards R.T. Qlon sl"V Res ij0Rse Cone Units Dev (Min) 1) 1,4-Dichlorobenzene-d4 11.77 152 /884531 20.00 ug/1 -0.14 19) Naphthalene-d8 15.37 136 3501657 20.00 ug/1 -0.15 31) Acenaphthene-dlO 20.66 164 164856'‘S 20.00 ug/1 -0.15 49) Phenanthrene-dlO 25.10 188 2365350' 20.00 ug/1 -0.14 59) Chrysene-dl2 33.13 240 1475983J 20.00 ug/1 -0.15 68) Perylene-dl2 37.24 264 1009277 20.00 ug/1 -0.18

System Monitoring Compounds 4) 2-Fluorophenol 0.00 112 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 5) Phenol-d5 0.00 99 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 6) 2-Chlorophenol-d4 11.77 132 536 0.01 ug/1 0.35 Spiked Amount 75.000 Recovery = 0.01% 7) 1,2-Dichlorobenzene-d4 12.28 152 9929 0.23 ug/1 -0.15 Spiked Amount 50.000 Recovery = 0.46% 20) Nitrobenzene-d5 0.00 82 0 0.00 ug/1 Spiked Amount 50.000 Recovery 0.00% 32) 2-Fluorobiphenyl 18.80 172 4086 0.04 ug/1 -0.01 Spiked Amount 50.000 Recovery = 0.08% 33) 2,4,6-Tribromophenol 0.00 330 0 •0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 62) Terphenyl-dl4 0.00 244 0 0.00 ug/1 Spiked Amount 50.000 Recovery = 0.00% Target Compounds Qvalue 2) Pyridine 0.00 79 0 N.D. 3) N-nitroso-dimethyl amine 0.00 74 0 N.D. 8) Phenol 0.00 94 0 N.D. 9) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 10) 2-Chlorophenol 0.00 128 0 N.D. 11) 1,3-Dichlorobenzene 0.00 146 0 N.D. 12) 1,4-Dichlorobenzene 0.00 146 0 N.D. 13) 1,2-Dichlorobenzene 0.00 146 0 N.D. 14) 2-Methylphenol 0.00 108 0 N.D. 15) 2,2'-oxybis(1-Chloropropan 0.00 45* 0 N.D. 16) 3&4-Methylphenol 0.00 108 0 N.D. 17) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 18) Hexachloroethane 0.00 117 0 N.D. 21) Nitrobenzene 12.97 77 207 N.D. 22) Isophorone 0.00 82 0 N.D. (#) = qualifier out of range (m) = manual integration 23263.D NP091101.M Thu Oct 11 12:13:24 2001 Page 1

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