GC/MS calibration data for TCLP method, Oct 2001

NYC 9/11 Public Portal Document

DFTPP Data File : C:\HPCHEM\1\DATA\OCT0201\DFTPP.D Vial: 1 Acq On 2 Oct 2001 12:19 pm Operator:. 2 09 GALOS Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01

Abundance TIC: DFTPP.D

ft 255553

255553

£55553

/V rime-> 24'40 24.60 2480 25'oO 25^20 25.40 25'60 25^80 26.00 26^20 26.40 26'60 26.80 27W 2^20 27^40 27.60 27.80 28.00 2820 Abundance Average of 26.346 to 26.392 min.: DFTPP.D 198 55553 250000 442

55553 69 127 255 152553 51 £5553 110 275 5553 224 L V-.-Mrt Xr T .'^,^^1 W J I. Illi. 24|1 I, ^?^31O3?3 346 365 333 403 423 0 3? Wtv I 'I 'I T I I T I 1' I J T I 13 j 11 ITy I T I I j 1 T T 1 |'1n 1 1 । T T 5 I । F1 1 T । i 1 1T । 1 1 I' r j 'I 1"l"1 |' *1 'I I ''I | I' 1 1' 1 | 1' j I"! । 1 1 । 1 । ”1 1 1 । j"*, j j 1 1 j i ■nfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 440

Spectrum Information: Average of 26.346 to 26.392 min. Target Rei. to Lower Upper Rei. Raw Result Mass Mass Limit% Limit% Abn% Abn Pass/Fail 51 198 30 60 34.8 114849 PASS 68 69 0.00 2 0.0 0 PASS 69 198 0.00 100 46.2 152532 PASS 70 69 0.00 2 0.0 0 PASS 127 198 40 60 46.0 151967 PASS 197 198 0.00 1 0.0 0 PASS 198 198 100 100 100.0 330155 PASS 199 198 5 9 6.5 21563 PASS 275 198 10 30 22.4 73816 PASS 365 198 1 100 2.3 7549 PASS 441 443 0.01 100 91.4 44146 PASS 442 198 40 110 75.9 250727 PASS 443 442 17 23 19.3 48320 PASS

DFTPP.D NP091101.M Wed Oct 03 09:13:05 2001

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