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GC/MS analysis results for sample AD22654, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD22654 conducted on October 12, 2001, noting other unknown compounds.

NYC-WTC_000087463–000087490

Folder label: “GC/MS Scan 9/19/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : C:\HPCHEM\1\DATA\OCT1101\22654.D Vial: 6 Acq On : 11 Oct 2001 2:38 pm Operator; 209 GTVLOS Sample : reinject Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Smoothing ; OFF Filtering: 5 Sampling ; 1 Min Area; 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location; TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation; 5

Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 5.126 3 9 35 rVB6 66693 477058 12.77% 1.729% 2 6.375 139 145 151 rBV2 22505 47201 1.26% 0.171% 3 6.476 151 156 167 rVV2 38454 100422 2.69% 0.364% 4 6.613 167 171 179 rW 21196 50985 1.36% 0.185% 5 6.723 179 183 197 rVB 28159 64962 1.74% 0.235% 6 11.626 711 717 726 rVB 29060 69014 1.85% 0.25.0% 7 11.763 726 732 744 rBV 1073870 2589889 69.31% 9.387% 8 15.371 1119 1125 1142 rBV 1576010 3630209 97.15% 13.158% 9 20.659 1694 1701 1715 rBV 1685668 3736689 100.00% 13.544% 10 25.084 2175 2183 2195 rBV2 1581789 3445152 92.20% 12.487% 11 27.324 2419 2427 2431 rBV 25063 49772 1.33% 0.180% 12 29.509 2658 2665 2673 rBV 459131 889834 23.81% 3.225% 13 29.628 2673 2678 2684 rW 122892 256266 6.86% 0.929% 14 29.748 2687 2691 2698 rW 67071 138307 3.70% 0.501% 15 30.702 2788 2795 2800 rBV 213428 424484 11.36% 1.539% 16 31.639 2 8 92 2 8 97 -2 903 rBV2 362129 740272 19.81% 2.683% 17 31.740 2903 2908 2917 rW 376633 783835 20.98% 2.841% 18 31.868 2917 2922 2927 rVB2 30784 64407 1.72% 0.233% 19 32.731 3010 3016 3023 rBV 408885 830005 22.21% 3.008% 20 33.126 3051 3059 3072 rBV2 1312655 3100691 82.98% 11.239% 21 33.383 3 093^087 3091 rVB 53164 106552 2.85% 0 .■3-86'% 22 33.686 3111 3120 3130 rBV 462645 990449 26.51% 3.590% 23 34.604 3215 3220 3228 rBV 346971 747788 20.01% 2.710% 24 35.127 3272 3277 3280 rBV 49133 110867 2.97% 0.402% 25 35.494 3312 3317 3329 rBV 298707 659334 17.64% 2.390% 26 36.357 3406 3411 3419 rBV 189144 420839 11.26% 1.525% 27 37.239 3498 3507 3511 rBV2 916176 2725716 72.94% 9.879% 28 38.359 3624 3629 3637 rBV3 49375 149970 4.01% 0.544% 29 39.607 3759 3765 3774 rVB2 34413 120441 3.22% 0.437% 30 42.058 4025 4032 4042 rBV3 14196 68261 1.83% 0.247%

NYC-WTC_000087469

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