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GC/MS analysis results for sample AD22656, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22656 conducted on October 11, 2001, identifying unknown compounds.

NYC-WTC_000087349–000087362

Folder label: “GC/MS Scan 9/19/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\l\DATA\SEP2801\22656.D Vial: 15 Acq On : 29 Sep 2001 2:10 am Operator: 209 GALOS Sample ; gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Smoothing : OFF Filtering: 5 Sampling : 1 Min Area; 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading -or trailing edge < 100 prefer < Baseline drop els^^angent > Peak separation: 5

Signal ; TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 6.385 142 146 153 rBV 30800 63226 1.75% 0.332% 2 6.495 153 158 168 rW 48464 125541 3.48% 0.660% 3 6.632 168 173 18 0 rW 23640 55222 1.53% 0.290% 4 6.743 181 185 194 rVB 31461 66915 1.86% 0.352% 5 11.645 714 719 729 rBV 29467 68559 1.90% 0.360% 6 11.783 729 734 75 0 rW 1019910 2576912 71.49% 13.550% 7 15.400 1122 1128 1144 rBV 1637189 3538620 98.17% 18.606% 8 20.688 1697 1704 1719 rBV 1661891 3604496 100.00% 18.953% 9 25.122 2179 2187 2198 rBV2 1498424 3373211 93.58% 17.737% io 33.164 3055 3063 3079 rBV2 1193939 2924031 81.12% 15.375%

11 37.286 3503 3512 3526 rBV2 896592 2621678 72.73% 13.785%

Sum of corrected areas: 19018411 22656.D NP091101.M Fri Oct 05 10:25:27 2001

NYC-WTC_000087355

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NYC-WTC_000087355Source: NYC Law Department, mirrored locally

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