GC/MS analysis report for sample AD22491, September 2001

Machine-extracted title · confidence 95%

Laboratory results for sample AD22491 indicating other unknown compounds detected via GC/MS on September 27, 2001.

NYC-WTC_000086808–000086817

Folder label: “508 Scan 9/15/01 9/26/01”

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OCR status: junk · source: pdftotext

NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : C:\HPCHEM\l\DATA\SEP2501\22491.D Vial: 2 Acq On : 25 Sep 2001 3:25 pm Operator: 2 09 G7VLOS Sample : GC/MS unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 6.381 142 146 152 rBV 20282 42431 1.25% 0.228% 2 6.492 154 158 169 rW 35947 90337 2.65% 0.486% 3 6.629 169 173 181 rW 16321 42251 1.24% 0.227% 4 6.740 181 185 193 rVB 24057 50147 1.47% 0.270% 5 7.759 293 296 307 rBV 61632 158833 4.67% 0.855%

6 11.642 713 719 729 rBV 25703 62837 1.85% 0.338% 7 11.789 729 735 746 rBV 935153 2393324 70.29% 12.881% 8 15.397 1122 1128 1147 rBV 1516468 3279966 96.34% 17.653% 9 20.684 1697 1704 1721 rBV 1578175 3404715 100.00% 18.325% 10 25.109 2179 2186 2195 rBV2 1375291 2984526 87.66% 16.063%

11 27.111 2399 2404 2409 rBV 28541 53539 1.57% 0.288% 12 28.791 2582 2587 2593 rVB 17492 35646 1.05% 0.192% 13 29.534 2663 2668 2673 rBV 84174 157230 4.62% 0.846% 14 29.654 2676 2681 2690 rVB 19115 39040 1.15% 0.210% 15 30.012 2715 2720 2724 rBV 32529 64611 1.90% 0.348%

16 30.728 2793 2798 2803 rBV 30981 63351 1.86% 0.341% 17 31.618 2890 2895 2898 rBV 63359 133976 3.94% 0.721% 18 31.673 2898 2901 2906 rW 76856 144172 4.23% 0.776% 19 31.765 2906 2911 2916 rW 61274 116966 3.44% 0.630% 20 32.757 3015 3019 3028 rBV 61415 128185 3.76% 0.690%

21 33.151 3052 3062 3067 rBV2 944375 2192792 64.40% 11.802% 22 33.216 3067 3069 3077 rVB 86280 173856 5.11% 0.936% 23 33.417 3086 3091 3096 rVB 103693 209354 6.15% 1.127% 24 33.720 3117 3124 3129 rVB 69952 148258 4.35% 0.798% 25 34.638 '3220 3224 3231 rVB 54175 111116 3.26% 0.598%

26 35.153 3276 3280 3287 rBV 68999 156348 4.59% 0.841% 27 35.529 3316 3321 3329 rBV 47356 102207 3.00% 0.550% 28 36.172 3386 3391 3395 rBV 55771 134546 3.95% 0.724% 29 36.227 3395 3397 3404 rVB 49871 108026 3.17% 0.581% 30 36.392 3411 3415 3423 rVB2 27447 61649 1.81% 0.332%

31 37.264 3503 3510 3524 rBV2 598648 1735472 50.97% 9.341%

NYC-WTC_000086815

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NYC-WTC_000086815Source: NYC Law Department, mirrored locally

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GC/MS analysis report for sample AD22547, September 2001 · Box DEP Box 67

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