GC/MS analysis results for sample AD22169, Sept 2001

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\l\DATA\SEP1901\22169.D Vial: 5 Acq On : 19 Sep 2001 6:44 pm Operator: GALOS Sample : GC/MS unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Sep 20 9:58 2001 Quant Results File: NP072501.RES Quant Method : C:\HPCHEM\1\METHODS\NP072501.M (RTE Integrator) Title : 208 625/TCLP calibration table 7/25/01 Cl IS 5 Last Update : Wed Jul 25 15:24:54 2001 Response via : Initial Calibration DataAcq Meth : HP060501

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.98 152 364225 20.00 ng/uL -0.02 19) Naphthalene-d8 15.59 136 1395685 20.00 ng/uL -0.03 31) Acenaphthene-dlO 20.87 164 644812 20.00 ng/uL -0.03 49) Phenanthrene-dlO 25.29 188 914984 20.00 ng/uL -0.02 59) Chrysene-dl2 33.29 240 634693 20.00 ng/uL -0.02 68) Perylene-dl2 37.40 264 447311 20.00 ng/uL -0.02

System Monitoring Compounds 4) 2-Fluorophenol 0.00 112 0 0.00 ng/uL Spiked Amount 75.000 Range 18 42 Recovery = 0.00%# 5) Phenol-d5 0.00 99 0 0.00 ng/uL Spiked Amount 75.000 Range 19 32 Recovery = 0.00%# 6) 2-Chlorophenol-d4 0.00 132 0 0.00 ng/uL Spiked Amount 75.000 Range 34 84 Recovery = 0.00%# 7) 1,2-Dichlorobenzene-d4 0.00 152 0 0.00 ng/uL Spiked Amount 50.000 Range 26 73 Recovery = 0.00%# 20) Nitrobenzene-d5 0.00 82 0 0.00 ng/uL Spiked Amount 50.000 Range 55 98 Recovery = 0.00%# 32) 2-Fluorobiphenyl 19.02 172 636 0.02 ng/uL 0.12 Spiked Amount 50.000 Range 42 78 Recovery = 0.04%# 33) 2,4,6-Tribromophenol 0.00 330 0 0.00 ng/uL Spiked Amount 75.000 Range 45 96 Recovery = 0.00%# 62) Terphenyl-dl4 0.00 244 0 0.00 ng/uL Spiked Amount 50.000 Range 58 98 Recovery = 0.00%# Target Compounds Qvalue 2) Pyridine 0.00 79 0 N.D. 3) N-nitrosodimethylamine 0.00 74 0 N.D. 8) Phenol 0.00 94 0 N.D. 9) bis(2-Chloroethyl)ether 0.00 93 0 N.D. t 10) 2-Chlorophenol 0.00 128 0 N.D. 11) 1,3-Dichlorobenzene 0.00 146 0 N.D. 12) 1,4-Dichlorobenzene 0.00 146 0 N.D. 13) 1,2-Dichlorobenzene 0.00 146 0 N.D. 14) 2-Methylphenol 0.00 108 0 N.D. 15) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 16) 3&4-Methylphenol 0.00 108 0 N.D. 17) N-Nitrosodi-n-propylamine 0.00 70 0 N.D. 18) Hexachloroethane 0.00 117 0 N.D. 21) Nitrobenzene 0.00 77 0 N.D. 22) Isophorone 0.00 82 0 N.D.

(#) = qualifier out of range (m) = manual integration 22169.D NP072501.M Thu Sep 20 09:58:49 2001 Page 1

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