GC/MS calibration table, Oct 2001

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\SEP2201\22490.D Vial: 3 Acq On : 22 Sep 2001 1:03 pm Operator; GALOS Sample : GC/MS unknown Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params; RTEINT.P Quant Time: Sep 24 15:16 2001 Quant Results File; NP072501.RES Quant Method ; C:\HPCHEM\1\METHODS\NP072501.M (RTE Integrator) Title ; 208 625/TCLP calibration table 7/25/01 Cl IS 5 Last Update ; Wed Jul 25 15:24:54 2001 Response via ; Initial Calibration DataAcq Meth : HP060501

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.99 152 374297 20.00 ng/uL -0.01 19) Naphthalene-d8 15.60 136 1431073 20.00 ng/uL -0.02 31) Acenaphthene-dlO 20.88 164 673940 20.00 ng/uL -0.02 49) Phenanthrene-dlO 25.30 188 969153 20.00 ng/uL -0.02 59) Chrysene-dl2 33.30 240 611635 20.00 ng/uL -0.02 68) Perylene-dl2 37.41 264 413427 20.00.ng/uL -0.02

System Monitoring Compounds 4) 2-Fluorophenol 0.00 112 0 0.00 ng/uL Spiked Amount 75.000 Range 18 42 Recovery = 0.00%# 5) Phenol-d5 0.00 99 0 0.00 ng/uL Spiked Amount 75.000 Range 19 32 Recovery = 0.00%# 6) 2-Chlorophenol-d4 0.00 132 0 0.00 ng/uL Spiked Amount 75.000 Range 34 84 Recovery = 0.00%# 7) 1,2-Dichlorobenzene-d4 0.00 152 0 0.00 ng/uL Spiked Amount 50.000 Range 26 73 Recovery = 0.00%# 20) Nitrobenzene-d5 0.00 82 0 0.00 ng/uL Spiked Amount 50.000 Range 55 98 Recovery = 0.00%# 32) 2-Fluorobiphenyl 19.03 172 666 0.02 ng/uL 0.13 Spiked Amount 50.000 Range 42 78 Recovery = 0.04%# 33) 2,4,6-Tribromophenol 0.00 330 0 0.00 ng/uL Spiked Amount 75.000 Range 45 96 Recovery = 0.00%# 62) Terphenyl-dl4 0.00 244 0 0.00 ng/uL Spiked Amount 50.000 Range 58 98 Recovery = 0.00%#

Target Compounds Qvalue 2) Pyridine 0.00 79 0 N.D. 3) N-nitrosodimethylamine 0.00 74 0 N.D. 8) Phenol 0.00 94 0 N.D. 9) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 10) 2-Chlorophenol 0.00 128 0 N.D. 11) 1,3-Dichlorobenzene 0.00 146 0 N.D. 12) 1,4-Dichlorobenzene 0.00 146 0 N.D. 13) 1,2-Dichlorobenzene 0.00 146 0 N.D. 14) 2-Methylphenol 0.00 108 0 N.D. 15) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 16) 3&4-Methylphenol 0.00 108 0 N.D. 17) N-Nitrosodi-n-propylamine 0.00 70 0 N.D. 18) Hexachloroethane 0.00 117 0 N.D. 21) Nitrobenzene 0.00 77 0 N.D. 22) Isophorone 0.00 82 0 N.D.

(#) = qualifier out of range (m) = manual integration 22490.D NP072501.M Mon Sep 24 15:18:16 2001 Page 1

NYC-WTC_000086620