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Method 200.8 ICP-MS lab results, NEWE samples, Jan 11, 2002

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ICP-MS analysis of water samples using Method 200.8 with elemental measurements (Be, Sc, Mn, In, Sb, Ho) and quality control replicates performed on January 11, 2002.

NYC-WTC_000085478–000085537

Folder label: “NEWE 1/11/2002 AD 31456 - AE00110 Batches 16390 16391 16402 copies made”

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NYC 9/11 Public Portal Document

Method 200.8 - Summary Report Sample ID: CCV STD2 60 PPB Sample Date/Time: Friday, January 11, 2002 15:44:34 Sample Type: Sample Sample Description: Number of Replicates: 3 Batch ID: Method File: d:\elandata\Method\NEWE200.8.mth Dataset File: d:\elandata\Dataset\daily performance\CCV STD2 60 PPB.2072 Sample Prep Volume (mL): Initial Sample Quantity (mg): Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Cone. Mean Cone. RSD Sample Unit r Be Sc-1 9 45 28098.649 592422.472 1.929 4.317 0.047 60.04454 5.58 ug/L 592422.472 ug/L L Mn 55 989634.094 1.353 1.672 57.95021 4.53 ug/L r: In 115 121 1213723.414 0.874 1213723.414 ug/L I Sb 465931.461 1.848 0.384 59.57429 2.27 ug/L L Sb 123 361968.977 1.711 0.298 60.30413 1.28 ug/L n Ho 165 1657051.685 1.811 1657051.685 ug/L L Tl 205 1524090.706 1.483 0.920 59.44995 0.41 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery I nt Std % Recovery Spike % Recovery Dilution % Diff Dup. Rei. % Diff r Sc-1 Be 9 45 93.303 L Mn 55 r> In 115 92.034 I Sb 121 L Sb 123 r> Ho 165 92.262 L Tl 205 Calibration Analyte MassCurve Type Correlation Coefficient f Be 9Linear Thru Zero 0.999992 |> Sc-1 45Linear Thru Zero L Mn 55Linear Thru Zero 0.999983 r> In 11 SLinear Thru Zero 1 Sb 121 Linear Thru Zero 0.999998 L Sb 123Linear Thru Zero 1.000000 r> Ho 165Linear Thru Zero L Tl 205Linear Thru Zero 0.999977

Sample ID: CCV STD2 60 PPB Report Date/Time: Friday, January 11,2002 15;45;06 Page 1

NYC-WTC_000085537

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