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Method 200.8 ICP-MS lab results, NEWE samples, Jan 11, 2002

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ICP-MS analysis of water samples using Method 200.8 with elemental measurements (Be, Sc, Mn, In, Sb, Ho) and quality control replicates performed on January 11, 2002.

NYC-WTC_000085478–000085537

Folder label: “NEWE 1/11/2002 AD 31456 - AE00110 Batches 16390 16391 16402 copies made

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NYC 9/11 Public Portal Document

Method 200.8 - Summary Report Sample ID: CeV STD1 30 PPB Sample Date/Time: Friday, January 11,2002 13:27:39 Sample Type: Sample Sample Description: Number of Replicates: 3 Batch ID: Method File: d:\elandata\Method\NEWE200.8.mth Dataset File: d:\elandata\Dataset\daily performance\CCV STD1 30 PPB.2039 Sample Prep Volume (mL): Initial Sample Quantity (mg): Aliquot Volume (mL): Diluted To Volume (mL):

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Cone. Mean Cone. RSD Sample Unit r Be 9 14530.418 1.918 0.024 30.28752 2.05 ug/L |> Sc-1 45 606299.017 2.217 606299.017 ug/L L Mn 55 519996.541 2.387 0.857 29.70913 3.30 ug/L r> In 115 1267695.534 1.447 1267695.534 ug/L I Sb 121 239714.720 0.194 0.189 29.34464 1.46 ug/L L Sb 123 184922.097 0.777 0.146 29.50090 2.16 ug/L r> Ho 165 1716049.251 1.592 1716049.251 ug/L L Tl 205 800386.965 3.105 0.466 30.14204 2.63 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery Int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rei. % Diff r Be 9 |> Sc-1 45 95.489 L Mn 55 r> In 115 96.127 I Sb 121 L Sb 123 r> Ho 165 95.547 L Tl 205 Calibration Analyte MassCurve Type Correlation Coefficient r Be 9Linear Thru Zero 0.999992 |> Sc-1 45Linear Thru Zero L Mn 55Linear Thru Zero 0.999983 r> In IISLinearThru Zero 1 Sb 121 Linear Thru Zero 0.999998 L Sb 123Linear Thru Zero 1.000000 r> Ho 165Linear Thru Zero L Tl 205Linear Thru Zero 0.999977

Sample ID: CeV STD1 30 PPB Report Date/Time: Friday, January 11,2002 13:28:12 Page 1

NYC-WTC_000085504

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