VOC analysis results, sample AE12738, June 4 2002

NYC 9/11 Public Portal Document

Data File C:\HPCHEM\l\DATA\02june04\0604Bl.D Vial: 1 Acq On 4 Jun 2002 12:16 pm Operator: 201-wb Sample lab blank Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\HP052902.M (RTE Integrator) Title VOCs BY EPA METHOD 524 Library C:\DATABASE\NBS75K.L

Peak Number 1 1-(Propenylthio)prop-l-ene Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

15.74 0.03 ug/L 22856 1,4-DIFLUOROBENZENE 15.09

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-(Propenylthio)prop-l-ene 114 C6H10S 000000-00-0 3 2 2,4-Imidazolidinedione, 3-methyl- 114 C4H6N2O21 006843-45-4 3 3 2,4,5-Trioxoimidazolidine 114 C3H2N2O31 000120-89-8 2 4 3-Cyclobutene-l,2-dione, 3,4-dihydr 114 C4H2O4 002892-51-5 2 Abundance Scan 690 (15.738 min): 0604B1.D (-) m/z 113.90 100.00% 1 4

Sigil

50 63 88 115.40 15.60 15.80 16.00 1T I ,44 , I , , , , I ,1, , ............................... 1 • . • • I.............. m/z 62.95 29.82% Tl/Z-> 40 50 60 70 80 90 100 110 120 Abundance #2940: 1 -(Propenylthio)prop-1 -ene 1 4 41 99

agga 15.40 15.60 15.80 16.00 m/z 88.00 27.40% 73 85 k 47 59 I ' I ' ' ’ ‘ I ' I ' -n/z-> 40 50 60 70 80 90 100 110 120 Abundance #64088: 2,4-lmidazolidinedione, 3-methyl- 1 4

T 15.40 15.60 15.80 16.00 58 m/z 49.85 17.91% 5000

86 42 71 ' I ‘ ' I ' '' I ‘ ' I ' ■n/z-> 40 50 60 70 80 90 100 110 120 Abundance #2824: 2,4,5-Trioxoimida2olidine ' I ' ' ' ‘ I ' ' 4|3 15.40 15.60 15.80 16.00 m/z 43.85 8.13%

114 5000 86

70 54 ___ [1, , , , , , , ........ I , I , ■n" 'n/z-> 40 50 60 70 80 90 100 110 120 15.40 15.60 15.80 16.00

0604B1.D HP052902.M Tue Jun 04 12:57:57 2002 Page 1

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