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VOC analysis results, sample AE12737, June 2002

Machine-extracted title · confidence 95%

Laboratory report for volatile organic compounds in sample AE12737 analyzed on June 3, 2002.

NYC-WTC_000083807–000083872

Folder label: “524 6/3/02

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Data File C:\HPCHEM\l\DATA\02JUNE3\0603Bl.D vial 2 Acg On 3 Jun 2002 10:31 am Operator 201-wb Sample lab blank Inst GC/MS Ins Mise Multiplr 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\HP052902.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library- : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Butane, 2-(ethenyloxy)-2-methy Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

15.74 0.03 ug/L 26174 1,4-DIFLUOROBENZENE 15.09

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Butane, 2-(ethenyloxy)-2-methyl- 114 C7H14O 029281-39-8 3 2 3-Pentanone, 2,4-dimethyl- 114 C7H14O 000565-80-0 3 3 4-Heptanone 114 C7H14O 000123-19-3 3 4 2,4-Pentanedione, 3-methyl- 114 C6H10O2 000815-57-6 3 Abundance Scan 690 (15.738 min): 0603B1.D (-) m/z 113.90 100.00% 1 4

5000

63 88 50 15.40 15.60 15.80 16.00 m/z 62.95 27.12% ' I ' ' ' ‘ I ' ' ' ' I ' 'n/z-> 10 20 30 40 50 60 70 80 .90 100 110 120 Abundance #3032: Butane, 2-(ethenyloxy)-2-methyl- 4)3

5000 15.40 15.60 15.80 16.00 55 71 m/z 88.00 26.43% 85 27 ' ■ I I I I 1 I I I Ji I , . I , I PI , ,1 . ' I ' ' ' ' I ' ' I 99 -tVr ' I ' ' ' ' I ' ' ' ' I ' ■n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #64142: 3-Pentanone, 2,4-dimethyl- 4)3

15.40 15.60 15.80 16.00 5000 71 m/z 49.95 20.34%

27 114 ......... .1....... ' ' ' I ' 55''' ' I ' ' ' ' II ' ' ' ' I ' ‘ ' I ' m/z-> 10 20 30 40 50 60 70 . 80 90 100 110 120 Abundance #3002: 4-Heptanone 43 15.40 15.60 15.80 16.00 71 m/z 43.90 5.27%

5000 27

114 15 58 86 99 I -n/z--> 10 20 30 40 50 60 70 80 90 100 110 120 15.40 15.60 15.80 16.00

0603B1.D HP052902.M Fri Jun 07 11:36:55 2002 Page 1

NYC-WTC_00008381 1

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NYC-WTC_000083811Source: NYC Law Department, mirrored locally

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