VOC analysis results, sample AE12737, June 2002

NYC 9/11 Public Portal Document Uuancicacion Keporc ^JMOC Keviewea; Data File C:\HPCHEM\l\DATA\02june3\0603B2.D Vial: 1 Acq On 3 Jun 2002 4:26 pm Operator: 201-wb Sample lab blank Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: GAS6.P Quant Time: Jun 3 17:04 2002 Quant Results File: HP052902.RES Quant Method : C:\HPCHEM\1\METHODS\HP052902.M (RTE Integrator) • Title :VOCs BY EPA METHOD 524 Last Update : Fri May 31 14:34:13 2002 Response via : Initial Calibration DataAcq Meth : HP052902

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-DIFLUOROBENZENE 0.00 114 0 0.00 ug/L -15.11 24) CHLOROBENZENE-D5 0.00 117 0 0.00 ug/L -21.75 52) 1,4-DICHLOROBENZENE-D4 26.95 152 1612 5.00 ug/L 0.02 System Monitoring Compounds 2) 1,2-DICHLOROETHANE-D4 0.00 65 0 0.00 ug/L Spiked Amount 5.000 . Recovery = 0.00% 3) 4-BROMOFLUOROBENZENE 0.00 174 0 0.00 ug/L Spiked Amount 5.000 Recovery = 0.00% 25) TOLUENE-D8 0.00 98 0 0.00 ug/L Spiked Amount 5.000 Recovery = 0.00% Target Compounds Qvalue 59) 2-CHLOROTOLUENE 25.09 91 7792 17.34 ug/L 95 60) 4-CHLOROTOLUENE 25.09 91 7792 17.34 ug/L 95 62) 1,2,4-TRIMETHyLBENZENE 25.81 105 7185 16.00 ug/L 88 64) P-ISOPROPYLTOLUENE 26.44 119 7444 18.01 ug/L 84 65) 1,3-DICHLOROBENZENE 26.80 146 8509 38.37 ug/L 93 66) 1,4-DICHLOROBENZENE 27.02 146 8250 35.64 ug/L 91 67) N-BUTYLBENZENE 27.32 91 12505 28.17 ug/L 95 68) 1,2-DICHLOROBENZENE 27.87 146 12230 66.20 ug/L 94 70) 1,2,4-TRICHLOROBENZENE 31.96 180 25561 233.48 ug/L 96 71) HEXACHLOROBUTADIENE 32.25 225 17480 235.80 ug/L 92 72) NAPHTHALENE 32.79 128 57012 249.49 ug/L 91 73) 1,2,3-TRICHLOROBENZENE 33.49 180 38523 453.14 ug/L 97 74) NITROBENZENE 29.86 77 11513 2609.00 ug/L 93

{#) = qualifier out of range (m) = manual integration 0603B2.D HP052902.M Mon Jun 03 17:05:03 2002 Page 1

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