VOC analysis results, sample AE12531, May 2002

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Data File : C:\HPCHEM\l\DATA\02may24\12531.D Vial: 3 Acq On : 24 May 2002 6:06 pm Operator: 201-wb Sample : 524 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP051702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Pealt Number 1 3-Hexanone, 2-methyl- Concentration Ranlc 3

R.T. .EstConc Area Relative to ISTD R.T.

15.80 0.04 ug/L 27213 1,4-DIFLUOROBENZENE 15.14

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexanone, 2-methyl- 007379-12-6 4 114 G7H14O 2 2-Oxepanone 000502-44-3 3 114 •C6H10O2 3 Butane, 2-(ethenyloxy)-2-methyl- 029281-39-8 3 114 C7H14O 4 2H-Pyran-2-one, tetrahydro-4-methyl 114 C6H10O2 001121-84-2 3 Abundance Scan 695 (15.801 min): 12531.D (-) m/z 114.05 100.00% 1 4 A 5000 63 88 L 57 15.40 15.60 15.80 16.00 16.20 ..... 44 yJ ...... . ...... m/z 62.95 40.10% n/z-> 20 30 40 50 60 70 80 90 100 110 120 Abundance #64192: 3-Hexanone, 2-methyl- 4|3 71

liWil I ' ' ' ' I ' ' 15.40 15.60 15.80 16.00 16.20 114 m/z 88.00 A 28.17%

55 99 ■ ...................... ' -n7z-> 20 30 40 50 60 70 80 90 100 110 120 Abundance #64123: 2-Oxepanone 42 515 ........... I ‘ ‘ ' I ' ‘ ' I -r-r-p-n-r-p-r 15.40 15.60 15.80 16.00 16.20 5000 m/z 57.05 . 19.46%

27 84 70 114

' I ' ' ' ' I •n/z--> 20 30 40 50 60 70 80 90 100 110 120 Abundance #3032: Butane, 2-(ethenyloxy)-2-methyl- 4)3 15.40 15.60 15.80 16.00 16.20 m/z 44.00 13.20%

5000 55 71 85 114 27 r I ' I ' ' ' ' I ' 1 99 ■n/z-> 20 30 40 50 60 70 80 90 100 110 120 15.40 15.60 15.80 16.00 16.20

12531.D HP051702.M Fri May 24 18:45:45 2002 Page 1

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