VOC analysis results, sample AE12279, May 2002

NYC 9/11 Public Portal Document

Data File C:\HPCHEM\l\DATA\02MAY23\0523Bl.D Vial: 1 Acq On 23 May 2002 8:55 am Operator: 201-wb Sample lab blank 1 (voc di) Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\HP051702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peale Number 2 Cyclotrisiloxane, hexamethyl- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 17.91 0.09 ug/L 77957 1,4-DIFLUOROBENZENE 15.05 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclotrisiloxane, hexamethyl- 222 C6H18O3Si3 000541-05-9 74 2 2-Methyl-7-phenylindole 207 C15H13N 000000-00-0 9 3 Arsenous acid, tris(trimethylsilyl) 342 C9H27AsO3Si3 055429-29-3 9 4 Pyrido[2,3-d]pyrimidine, 4-phenyl- 207 C13H9N3 028732-75-4 5 Abundance Scan 818(17.911 min): 0523B1.D (-) m/z 207.15 100.00% 2(117

5000

96 133 17.60 17.80 18.00 18.20 44 I m/z 208.15 24.22% -n/2-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #70586: Cyclotrisiloxane, hexamethyl- 2(1)7

5000 17160 17180 18.00 18.20 m/z 96.10 16.50% 96 133 75 I 115 I , 177 [ I" " I rTTpnT-tp-TTTYTTThyrrTTyVT^^ I'''' I Tri/2-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #24652: 2-Methyl-7-phenylindole 2(1)7

__!A6p_1Y8p_18W_18;20__ 5000 m/z 209.15 14.18%

30 102 f tV2-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #48300: Arsenous acid, tris(trirnethylsilyl) ester 2( )7 T 17.60 17.80 18.00 18.20 m/z 191.10 12.15%

5000

73 105 133 44 Il .1 I. 327 239 I" Ti/2-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 17.60 17.80 18.00 18.20

0523B1.D HP051702.M Tue May 28 08:42:13 2002 Page 2

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