VOC analysis results, sample AE12279, May 2002

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Data File C:\HPCHEM\l\DATA\02MAY23\12278F.D Vial: 12 Acq On 24 May 2002 2:20 am Operator: 201-wb Sample nys; fb Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP051702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peale Number 2 Cyclotrisiloxane, hexamethyl- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

17.96 0.05 ug/L 38970 1,4-DIFLUOROBENZENE 15.12

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclotrisiloxane, hexamethyl- 222 C6H18O3Si3 000541-05-9 64 2 2-Methyl-7-phenylindole 207 C15H13N 000000-00-0 9 3 Pyrido[2,3-d]pyrimidine, 4-phenyl- 207 C13H9N3 028732-75-4 5 4 IH-Indole, 5-methyl-2-phenyl- 207 C15H13N ' 013228-36-9 5 Abundance Scan 822 (17.962 min): 12278F.D (-) m/z 207.15 100.00% 2(1)7

5000

96 191 17.60 17.80 18.00 18.20 44 I m/z 208.15 24.26% m/2-> 20 40 ' I ' ' ' ‘ I ' 60 80 100 120 140 160 180 200 h Abundance #70586: Cyclotrisiloxane, hexamethyl- 2(1)7

5000 17.60 17.80 18.00 18.20 m/z 96.00 17.21%

75 119 147 163 177 •n/z-> 20 40 60 80 100 120 140 160 180 200 Abundance #24652: 2-Methyl-7-phenylindole 207

17.60 17.80 18.00 18.20 m/z 209.15 16.93% 5000 4

30 102 I-, I-, 76 88 I, 178 , ■n/2-> 20 40 60 80 100 120 140 160 180 200 Abundance #24634: Pyrido[2,3-d]pyrimidine. 4-phenyl- ,,, 2(1)7 I ' ' ' 17.60 17.80 18.00 18.20 m/z 191.10 15.72%

5000 179 77

•Ti/z-> 20 ........ X 40 60 80 100 120 140 160 180 200 17.60 17.80 18.00 18.20

12278F.D HP051702.M Fri May 24 14:58:03 2002 Page 2

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