VOC analysis results, sample AE10890, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\02MAY07\10900.D Vial: 6 ■ Acq On 8 May 2002 12:50 am Operator: 201-wb Sample nyc . Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\HP042202.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Cyclobutene-l,2-dione, 3,4-d Concentration Rank- 1

R.T. EstConc Area Relative to ISTD R.T.

15.78 0.03 ug/L 25332 1,4-DIFLUOROBENZENE 15.12

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Cyclobutene-l,2-dione, 3,4-dihydr 114 C4H2O4 002892-51-5 4 2 1,3-Dioxolan-2-one 88 C3H4O3 000096-49-1 4 3 Hydrazine, 1,2-diethyl- 88 C4H12N2 001615-80-1 4 4 3-Hexanone, 2-methyl-114 C7H14O 007379-12-6 4 Abundance Scan 694 (15.784 min): 10900.D (-) m/z 114.15 100.00% 1 4 8000

6000

4000 ■^~r

RQ________88I____________ 15.40 15.60 15.80 16.00 _44_____ 88 m/z 88.10 27.04% m/z-> Abundance ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ‘ 10 20 30 40 50 ' I ' ‘ 60 ' I ‘ 70 #2826: 3-Cyclobutene-l,2-dione, 3,4-dihydroxy- ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' 80 90 100 110 120 ' ' I ' ft 29 58

5000 114 15.40 15.60 15.80 16.00 m/z 62.95 23.15% 86 17 40 .... ,68....I...... Tl/Z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #62892: 1,3-Dioxolan-2-one 2|9

15.40 15.60 15.80 16.00 5000 43 m/z 44.00 20.72% 88

rj-i-T-r-r-p--r-rJj-rT-T-r^ ' I ' ' ' I I ' ' ' ' I ' ‘ ' I ' •n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #840: Hydrazine, 1,2-diethyl- 3|1 15.40 15.60 15.80 16.00 59 88

liliW 44 73

' I' ‘ ‘' I' J. Ill.. I,. ,1.. ... •n/z-> 10 20 30 40 50 60 70 80 90 100 110 120

10900.D HP042202.M Wed May 08 09:35:16 2002 Page 1

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