VOC analysis results, sample AE10240, May 3, 2002

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Data File C:\MSDCHEM\l\5973N\02MAY03\10240D.D Vial: 18 Acq On 3 May 2002 11:21 pm Operator: Sample nyc Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSC.P Quant Method : C:\MSDCHEM\1...\W050302.M (RTE Integrator) Title : VOC method 8260 Library : C:\DATABASE\WILEY7N. L * * * * *.* *************************************************************** Peak Number 5 4-(Prop-2-enoyloxy)octane Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

33.79 0.03 ug/L 19178 1,4-Dichlorobenzene-d4 31.54 Hit#.of 5 Tentative ID MW MolForm CAS# Qual ----- i.. 1 4-(Prop-2-enoyloxy)octane 184 C11H20O2 000000-00-0 47 2 5-Etiiyl-l-nonene 154 C11H22 019780-74-6 43 3 Heptanal 114 C7H14O 000111-71-7 43 4 Heptanal (CAS) $$ n-Heptanal $$ ... 114 C7H14O 000111-71-7 43 'Abundance Scan 3035 (33.793 min): 10240D.D (-) m/z 7 07100 100.00% 43 70

523 55 112 95 121 207

0 1 -rfTT 1 " ' ‘ I I 33.40 33.60 33.80 34.00 34.20 m7z 437175 91747% ■n/z-> :20 30 40 50 60 70 80 90 100110120130140150160 170180 190 200 210 ■(4 Abundance! . #92785; 4-(Prop-2-enoyloxy)octane 55 70

5000 M n A 33 40 33.60 33.80 34.00 34.20 42 83' 112 “fn/z 44.00 64.34% 156 0^ I " " I' " ' I I'''' I j r,-| r I 1 I . I I . H . I 1 , . I I

20 30 40 50 60 70 80 90 100110120130140150160 170180190 200 210 Abundance! #53730: 5-Ethyl-1-nonene 5)5 73

33.40 33.60 33.80 34.00 34.20 5000 in/z 55.20 46.98% “ 97 112

125 154 0^ I' I ‘ • I' ■ 111" " I I" " I I" '' 1 ‘‘' I TiZz-> ;20 30 40 50 60 70 80 90 100110120130 140150160 170180190 200 210 Abundance! #15197: Heptanal A tJ 44 ja40_3a60_ja80_J<00_34^ 70 m/z 57720 42.17% 27 55 5000

96 0 ............... T U ‘ " I' ‘ ‘ I' " ' I' ' " I " " I " " I 20 30 40 50 60 70 80^ 100 110 120 130 140 150 160 170180 190^0210 33.40 33.60 33.80 34.00 34.20

10240D.D W050302.M Mon May 06 12:26:43 2002 Page 7

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